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Petr Vavruch: The correct lubricant

Textbook and ready reference book - See comments about the book

Download the updated version of the book (minor revision dated 20 February 2021, 2.1 Mb)

Should you wish to make a contribution towards this project, you can buy another copy of the book (the first revision) here

To say lubrication is important is an understatement. The role of lubrication in reducing friction, cooling, minimising wear, improving efficiency and avoiding unplanned downtime is as critical as the design or componentry of any machinery.
Aaron Stone

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Petr Vavruch also presents a two-day workshop anywhere in the world for US$1000 plus the necessary moderate expenses

See comments by the participants of the workshops

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This web page provides additional information and illustrations (Petr Vavruch does not always agree with all the views expressed in these web sites)

Please click here to report any addresses that no longer work or to suggest additional web sites

NEWS

George Gill - Conductive deposits pose threats to EVs (21 April 2021)
Mike Kunselman - Does new OEM global fluids consortium spell end of ILSAC? (14 April 2021)
ACEA revisions progressing (13 April 2021)
Tim Sullivan - OEMs propose global system for specs (13 April 2021)
Valvoline launches new premium full synthetic motor oil (6 April 2021)
Dr Raj Shah, Dr Steve Nitodas, Isaac Kim - Nano-additives show promise in reducing friction and wear (17 March 2021)
Electrified efficiency: ZF offers 800-volt components for electric vehicles (11 March 2021)
Dr Neil Canter - Preparation of base oils from plastic resins (March 2021)
Christoph Rofka, Deepak Davendrappa, Jacob Sterlin and Rashpal Bhatti - Marine diesel engines: The beginning of the end? (23 February 2021)
How organizations are reducing losses due to preventable maintenance issues (18 January 2021)
FLUKE - Root causes of lubrication degradation (webinar, 2021)
Petro-Canada's factory fill for Allison’s TES 668TM specification (19 January 2021)
International Maritime Organization legislation update (12 January 2021)
Sediment concerns in marine fuels (7 December 2020)
Dr Raj Shah, Dr Ken Hope, Nathan Aragon - Fuel economy considerations: Effect of lube oils and their volatility (November 2020)
Proposed ASTM standard aims to provide accurate information on hydrocarbons (2 November 2020)
Leandro Benvenutti, Infineum - New transmission fluid challenges (27 October 2020)
Ryan Martin and Dominique Bonte - Digital transformation what is new, what is next and what it all means (October 2020)
Wolf Oil launches engine oils that meet Renault’s RN17 lube specs (18 June 2020)
HYZON Motors opens Europe’s first dedicated hydrogen truck plant (1 October 2020)
Hyundai ships world’s first mass-produced fuel cell heavy-duty trucks (1 October 2020)
Red Line Synthetic Oil launches new chain lube (1 October 2020)
Castrol launches new pre-oil change treatment product (1 October 2020)
Breakthrough diesel exhaust fluid (1 October 2020)
Bryan Allison - Rolling element bearings development (October 2020)
Allison announces new ATF spec for on-highway equipment, TES 668 (29 September 2020)
Proposed ASTM standard will help determine methyl hydrogen content in base oils (29 September 2020)
Top five automotive industry trends (15 September 2020)
Tribology trends and challenges in electric vehicles (14 September 2020)
Jeanna Van Rensselar - Lubrication and tribology trends (and challenges) in electric vehicles (13 July 2020)
Dr Raj Shah, Dr Hind Abi-Akar, Stanley Zhang - Modern global engine oil standards (September 2020)
Porsche says combustion engines still viable with synthetic fuels (8 September 2020)
Chevron Marine Lubricants' white paper with findings how ship operators manage the transition from high-sulphur fuel oil (HSFO) to very low-sulphur fuel oil (VLSFO) (28 August 2020)
Managing waxy marine fuels (August 2020)
Mary Moon - NLGI unveils new grease specs (8 July 2020)
Hyundai’s first mass-produced fuel cell heavy-duty trucks (8 July 2020)
Caitlin Jacobs - Upping the ante on food-grade lubes (6 May 2020)
ILSAC GF-6A, GF-6B, and API SP engine oil products on the shelf starting today (4 May 2020)
API opens early applications for licensing of ILSAC GF-6A, GF-6B, and API SP engine oils (11 March 2020)
Lutz Lindemann - Alternatives to electrification 'politically neglected' (21 February 2020)
Mary Beckman - The business of truck lubrication (February 2020)
STLE presentations by Afton, Croda, Evonik, ExxonMobil, King Industries, LANXESS (prev, Ciba), Münzing, Lubrizol (2019)
Lubrizol white paper identifies VLSFO engine condition challenges (11 January 2020)
Tim Sullivan - Balancing viscosity, wear in HDEOs (8 January 2020)
GKN Automotive launches strategy to make electric propulsion more affordable (20 December 2019)
GM releases Dexos1 Gen 3 details (18 December 2019)
ENGIE and Anglo American to develop first hydrogen-powered mining haul truck (November 2019)
BorgWarner develops innovative torque-vectoring dual-clutch gears for electric vehicles (6 November 2019)
David Tsui - Additives manufacturers brace for change (November 2019)
Rachel Fowler - Formulators are working with an increasingly smaller portfolio of available biocide chemistries (November 2019)
Petronas to launch an IPO for South Africa’s largest fuel retailer Engen (5 October 2019)
Nynas introduces world’s first bio-based high-performance transformer fluid (4 October 2019)
Mary Beckman - Today’s automatic transmission fluids (October 2019)
Infineum - Are all lubricity products equal? (25 September 2019)
Pei Yi Lim, Infineum - Emissions regulations impact motorcycles (24 September 2019)
Jeanna Van Rensselar - Sea change for marine fuels and lubricants (September 2019)
Astron Energy is a leading supplier of petroleum products in South Africa
NCWM amends Tractor hydraulic fluid section of NIST Handbook 130 (19 July 2019)
The International Maritime Organization (IMO) has approved and adopted a comprehensive set of guidance and guidelines to support the consistent implementation of the lower 0.50% limit on sulphur in ships' fuel oil (19 July 2019)
Marine lubricants will need formulations for multiple types of fuel when ship owners comply with IMO 2020 regulations (19 July 2019)
JASO is preparing a new PCMO specification for ultra-low-viscosities 0W-12 and 0W-8 (19 July 2019)
Japan’s ultra-low viscosity passenger car motor oil specification GLV-1 will impacts base oil quality demands (12 July 2019)
IMO 2020 Sulphur Cap Regulations and marine lubricants (TLT Sounding Board, July 2019)
Test your knowledge: 3 questions
Electric vehicles (links)
World’s first CTL base oil plant starts production in Shanxi Province, China (24 May 2019)
George Gill - Low viscosity oils called challenge to industry (26 March 2019)
BMW and Daimler create a global player to provide sustainable urban mobility (28 February 2019)
Michael D. Holloway - Using drones for remote oil sampling (August 2018)
GE exits locomotive business, sells division to Wabtec (28 May 2018)
Mazda Motor to launch world’s first commercial gasoline engine to use compression ignition (9 August 2017)

Graphene, a recently discovered material, is defined as a form of elemental carbon composed of a single flat sheet of carbon atoms arranged in a repeating hexagonal lattice. This lacy, honeycomb-like sheet of carbon atoms — essentially the most microscopic shaving of pencil lead you can imagine — is not just the thinnest material known in the world, but also incredibly light and flexible, hundreds of times stronger than steel, and more electrically conductive than copper.

The latest research interacts (a) molybdenum disulphide with nano-diamond particles on one surface and (b) a diamond-like carbon (DLC) surface on a ball to determine if superlubricity could be detected in a similar manner to graphene. It works by breaking moly and creating a onion-like carbon structure.

SUBJECT LINKS FOLLOWING THE SECTIONS OF THE BOOK

Lubrication - general
1. Three basic aspects of lubricating oils
1.1 Viscosity, kinematic, dynamic, ISO VG
1.2 and 1.3 Viscosity of engine oils and automotive gear oils, SAE, multi-grade
1.4 Viscosity index, viscosity modifiers, viscosity-temperature chart, calculators
1.5 Pour point, pour point depressant
1.6 Flash point and Noack volatility
1.7 Charts, blending
Answers to 1.7 (link)
1.8 Foam, entrained air and air release, defoamant
1.9 Base stocks, saturates, aromatic hydrocarbons, API groups
1.9.1 What does 'synthetic' mean?
Synthetics - usage
1.9.2 Polyalphaolefins (PAO)
Food-grade lubricants
1.9.3 Other synthetic hydrocarbons
1.9.5 Polyalkylene glycols (PAG) (polar compounds)
1.9.6 Esters, amides, environmentally friendly lubes
Vegetable oils and biodegradable lubricants
1.9.7 Naphthenics
1.10 Oil performance, performance additives
1.11 Water separability (demulsibility)
1.12 Supplemental ('proprietary') additives
2. Answers to REVISION 1 (link)
3.1 Engine oils, detergents, dispersants, ZDDP, fuel economy
Friction and wear
Sludge, drain intervals, maintenance
3.2 Engine oil specifications, API service categories
3.3 and 3.4 Sulphated ash, TBN
3.5 ILSAC (International Lubricant Standardization and Approval Committee)
3.6 ACEA (Association des Constructeurs Européens d'Automobiles) and Equipment Manufacturers (OEM)
3.9 Two-stroke petrol engines
3.10 Outboard motor oils
3.11 Motorcycle oils
Electric vehicles
3.12 Gas engines
3.13 Marine engines and emergency power generation, marine lubes
3.15 Gas turbines
3.16 Automotive gear oils for manual gearboxes
3.17 Limited slip differentials
3.18 and 3.19 Eaton (form. Fuller) and ZF-FreedomLine, Caterpillar
3.20 Allison
3.21 Total Acid Number (TAN)
3.22 Automatic transmission fluids (ATF)
3.23 Farm equipment oils, UTTO, STOU
3.24 Brake fluids
4. Answers to REVISION 2 (link)
5. Lubrication conditions, EHL, anti-wear, EP
6. Industrial gear oils
Micro-pitting, wind turbines and using synthetics in gears
6.1 Worm gears (PAG)
6.3 Open gears
Gear failures
Chain and wire rope lubrication
7. Greases (also 7.3, 7.5 and 7.7)
Grease guns and systems
7.1 and 7.2 Grease thickeners, polymers and compatibility
7.4 Grease lubricated rolling element bearings
7.6 Grease-filled gearboxes
7.8 Grease or oil?
8. Bearings (also 8.2)
Paper machines, spindle oils, sugar mills, Morgan and Danieli
8.1 Rolling element bearings
Rolling element bearing failures
8.4 Steam turbines, varnish
9.1 Air compressors, coalescer filters
9.2 Vacuum pumps
9.3 Compressors for other gases
9.4 Refrigeration compressors
10. Hydraulic fluids
10.1 Fire-resistant fluids
10.2 Oil cleanliness
Particle counting, cleaning oil, filtration
Oil filters
Flushing
11. and 13. Lubricant storage and storage life (shelf life)
12. Transformer oils
14. Machine tools
15. Cutting fluids, metal cutting, grinding
16. Rust preventives
17. Answers to REVISION 3 (link)
Hint No. 2 for CHALLENGE (link)
Hint No. 3 for CHALLENGE (link)
18. CHALLENGE solution (pdf)
Answers to questions (link)
Oil suppliers' information, approved and recommended lubricants (for information only)
Maintenance, lubricant monitoring, sampling and analysis (in the following sections)
Monitoring equipment without special instruments and without laboratory samples
Designing oil analysis programme, condition monitoring, standard test methods
Oil and grease sampling
Sampling frequencies
Advanced test methods
Root causes of failures, analysis interpretation
Grease analysis
Oil cleanliness
Particle counting, cleaning oil, filtration
Oil filters
Flushing
Water contamination
Fuels
Maintenance strategies - reactive, preventive, predictive and proactive
Management, maintenance management, Total Productive Maintenance
Reliability, RCM
Maintenance/Industry 4.0, Internet of things (IoT), AI, CMMS
Lubrication practices, lubrication excellence
Training, education, skills
Light reading

In machinery condition monitoring, a decision on the condition of a machine is dependent on the nature of its signals. For example, if the machine produces excessive noise and vibration, one gets a clue that something is not normal with the machine. These signals are usually time varying and need to be understood because they carry the information from the machine to the decision system, which can be a developed software or a person.
Machinery Condition Monitoring: Principles and Practices

In the lubrication industry it is pretty common to have heard of or experienced a lubrication issue due to mixing of incompatible lubricants. Issues encountered include excessive foaming, formation of precipitates or deposits and loss of key performance characteristics such as water separability. Given the gravity of the impact on machine reliability that these issues can cause, there is a demand for testing that can help predict if mixing two lubricants might result in operational issues. Although the lubricants may be deemed equivalent or comparable, that does not mean they are compatible.

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Are you having machine failures? Most companies are now realizing that maintaining clean oil is one of the best investments they can make, with contamination at the core of premature machinery failure and diminished lubricant life. A desiccant breather can be used as a first line of defence in preventing contaminants from ruining your equipment.

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Ninety percent of lubrication professionals say a lack of attention has negatively impacted the reliability of equipment at their plant.

1. Three basic aspects of lubricating oils

What is lubrication?
Lubrication basics
Wikipedia - Lubricant
Lubricants
MRG Labs - Laboratory Lubricant Analyst training (LLA-I) clip
Effects of using a wrong lubricant (2018)
Jim Fitch - Viscosity starved machines (2015)
David Wedlock - Uninhibited base oils (2017)
Oxidation (TOST) test description (Shell Tellus S)
How oxidation occurs (short video)
Antioxidants
Dr Robert M. Gresham - Antioxidants (2018)
Vincent Bouillon, BfB Labs - Overview of oxidation laboratory tests on industrial lubricants (first published in Lubes magazine, 2017, 1.3 Mb)
Joshua Jurs, PhD, Global Industrial Oil Technical Manager, Vanderbilt Chemicals LLC - Long term testing of antioxidants for industrial applications (turbine) in Group I and II base oils (first published in Lubes magazine, Feb 2019, 1.6 Mb)

According to hydraulic component manufacturer Danfoss, if a hydraulic system operates at 85 °C, oil life is just 12% of what it would be if the system operated at 60 °C. And if the system operates at 100 °C, oil life is only 3% of what it would be if the system operated at 60 °C.

Some antioxidants, such as butyl hydroxy toluene (BHT), will turn oil bright red when oxidizing during normal service. While not always cause for alarm, it is clear evidence that the antioxidant is depleting.

Oxidation test RBOT
Mohammad Naseer Uddin - Misconceptions about RPVOT costing companies millions US$ (2018)
Schaeffer - Oxidation and new requirements for Heavy-Duty Diesel (HDD) oils (2017)
Dr Robert M. Gresham: Rust (2018)
Rust and corrosion
Inhibiting rust and corrosion to prevent machine failures
Dr Nancy McGuire - Sulphur-based additives (2018)
Dr Neil Canter - Metalworking fluids: Update on boundary lubricity additives (2021)

1.1 Viscosity, kinematic, dynamic, ISO VG

Simon Michell - Oil viscosity made simple (2020)
Art Gatenby - Shear stress and shear rate (2020)
Drew Troyer: Kinematic viscosity (2002)
CSC - What is the difference between dynamic and kinematic viscosity? (2015)
Learn Oil Analysis - Viscosity of lubricating oils (video 2017)
Dynamic viscosity explained (video 2014)
Parker Kittiwake - Viscosity: A lubricant’s most important characteristic
LE - Viscosity
Oelcheck - Viscosity
Synlube - Viscosity
TLT - Viscosity and types of fluids (2017)
Oil viscosity, how it's measured and reported
Cannon Instrument - Measuring viscosity of industrial and engine oils (one page, 2017
Drew Troyer - Understanding absolute and kinematic viscosity (2002)
ISO VG limits
Noria - ISO VG limits
Industrial lubricants (incl. Viscosity guides)
Brendan Casey - Viscosity of hydraulic fluids
Roymech - Viscosity theory
Viscosity, temperature and pressure
Gear oil viscosity calculation (theory, 2018)
Viscosity too high, too much lubricant (short video, 2018)
Affordable viscosity tester
Parker Kittiwake - Heated viscometer
Spectro - Portable kinematic viscometers
Dr Nancy McGuire - Calculating lubricant viscosity versus temperature (theory, 2021)

dynamic viscosity definition

Viscosity is a fluid's characteristic demonstrating its resistance to flow. By definition, unit of dynamic ("absolute") viscosity is the poise, which is defined as the force in dynes required to move a surface one square centimetre in area past a parallel surface at a speed of one centimetre per second, with the surfaces separated by a fluid film one centimetre thick. We commonly use the centipoise (cP) and for kinematic viscosity the centistoke (cSt). There are other methods for determining viscosity, including Saybolt Universal Viscosity (SUV), Saybolt Furol viscosity, Engler viscosity, and Redwood viscosity. Since viscosity varies inversely with temperature, its value is meaningless until the temperature at which it is determined is reported. Viscosity can increase by oxidation and can be reduced by heating through thermal cracking.

1.2 and 1.3 Viscosity of engine oils and automotive gear oils, SAE, multi-grade

Boris Zhmud - Viscosity matters (2019)
Lubricant must perform and properly flow, even at the coldest temperatures (2018)
JC Motors - Understanding motor oil viscosity
Lubrizol - High temperature high shear viscosity test
SAE adds two new grades SAE 8 and 12 to J300
SAE adds light engine oils categories
Ultra-low viscosity engine oils - Go to page 26
Widman - SAE J306 Viscosity classification for automotive gear oils
Brookfield instrument manual
Brookfield: More solutions to sticky problems (2017)
Early discussion about new SAE grades
Japanese race to reduce viscosity

In America, fortunately only there, they have a disgusting ignorant slang calling SAE numbers "weights", like "30 weight" or "10w30 weight". I suggest that you use it only if you want to show that you know NOTHING about lubricants.

Ford recommends using SAE 5W-50 viscosity grade for its GT-500 engine instead of the SAE 5W-20 or SAE 5W-30 used by other engines.
Arup Gangopadhyay

A small increase in lubricant viscosity may be due to the volatilization of base oil "lighter ends" after prolonged high-level operation (i.e. the lubricant has become "thicker"). Significant increases in viscosity up to 20 percent are regarded as severe, caused by incorrect addition of a higher viscosity lubricant, extensive soot contamination and base oil oxidation.

1.4 Viscosity index, viscosity modifiers, viscosity-temperature chart, calculators

Trevor Gauntlett - The value of VI (2021)
tribonet - Viscosity index (2019)
Viscosity index (short video)
Wikipedia - Viscosity index
TLT - Viscosity index improvers (2011)
Don't ignore viscosity index (2012)
Viscosity modifiers: A fundamental study
Viscosity index improvers
Afton - HiTEC 5708A VI improver/Pour point depressant
Chevron Oronite OCP viscosity modifiers
Evonik - Viscosity modifiers
Evonik - VISCOPLEX VIIs for transmission fluids
Functional products viscosity modifiers
Infineum - Viscosity modifiers
Lubrizol - Viscosity modifier calculator
Widman - VI and viscosity calculators
A2 size nomogram for viscosity index

Applicable range of the above nomogram:
This graph is designed for viscosity indexes between 0 and 100, viscosity of 2-20 cSt at 100 °C, and 6.4-495 cSt at 40 °C. I will publish the wider range graphs (up to VI=200 and viscosity of 2-50 cSt) in near future.
Instruction: This graph has 12 graded lines for viscosity and one for viscosity index. Six lines are nominated for viscosity at 100 and six for 40 centigrade that are paired with letters A, B, C, D, E, and F. To start with the graph:
1. Determine the kinematic viscosity (in cSt) at 100 °C on one of the curved graphs and highlight it with a dot.
2. Determine its paired line using the letters bellow the graph.
3. Find the viscosity at 40 °C on its pair and highlight it with the second dot.
4. Draw a straight line with two dots and using a ruler, and extend it to right hand side to intercept the "Viscosity Index" line.
5. The VI is the interception point of these two lines. You can report it with ±1 accuracy.
6. If you have limitation to measure viscosity at 40 and 100 °C, use ASTM D341 to estimate them.
M. Mahdi Karima

In 1929 Dean and Davis devised a system to express the viscosity/temperature relationship of an oil. The system, viscosity index (VI), was based on the viscosities of base oils obtained from a paraffinic Pennsylvanian crude oil, which was arbitrarily assigned a VI of 100, and base oils obtained from a naphthenic Gulf Coast crude oil, which was assigned a VI of 0.

ASTM D2270 - VI calculator
Calculator: Viscosity at operating temperature
Calculator: Viscosity at operating temperature
Calculator: Viscosity at operating temperature

1.7 Viscosity-temperature chart, blending

A proper viscosity-temperature chart
Various viscosity-temperature charts
Blending calculator
Widman - Mixing oils
Viscosities of base oil blends (spreadsheet)

1.5 Pour point, pour point depressant

Pour_point and pour_point depressants
Wikipedia - Pour point
Evan Zabawski - Pour point (discussion, 2019)
Engineers Edge - Pour_point
Noria - When to use an oil heater (2016)
Oronite - Pour_point depressants
Afton - Pour_point depressants (see video)
Evonik - Pour_point depressants
Oil gelation (2016)

1.6 Flash point and Noack volatility

Wikipedia - Flash_point
Noack_volatility_test (but it is done at 250 °C !!)
Volatility of synthetic and mineral oils using TGA
Noack volatility test: a new set of upheavals (2018)
Flash point and fire point

Volatility of engine oil lubricants in service has become of increasing concern to equipment manufacturers because of oil consumption, engine deposits and air pollution effects. Two types of methods are used to assess volatility: The first is based on simulated distillation by gas chromatography (GCD), and the second, Noack volatility, measures bulk oil weight loss after heating at a prescribed temperature/time.

1.8 Foam, entrained air and air release, defoamant

The polar nature of engine oil additives gives rise to their foam-stabilizing properties. The splashing action or the mechanical agitation, or both, of the crankcase oil during engine operation causes air and other vapors to be whipped around, resulting in foam generation. In extreme cases, the oil actually can be lost because of the foam. The entrainment of the air in the oil can also decrease the ability of the oil to provide an effective hydrodynamic lubricating film because of the air bubbles that compromise the integrity of the film.

Defoamants are typically polydimethyl siloxanes of various molecular weights and are only required at a few parts-per-million concentration to control lubricant foaming. It should be noted that the siloxanes are dispersed in the lubricant in the form of small particles or globules with specialized equipment. These small particles can be seen through the use of a phase contrast microscope similar to that used in clinical laboratories.

Cavitation is a violent condition typically in the suction of a pump leading to wear caused by air bubbles or water or oil vapour bubbles.

Finding the cause of foam in oil (short, 2019)

Bad article, confusing foam with air entrainment. Petr: Don't add defoamant unless you really have to.

Is air a contaminant? (2008)
How foam impacts lubricant health (short, 2017)
TESTOIL - Foaming tendency test
Foaming and air dispersions in industrial gear oils (2015)
More stable foam is due to differential evaporation of the multicomponent base oils (2018)
Foaming and air entrainment (comment, 2018)
Controlling oil aeration and foam (brief)
Causes and solutions for foaming in oil (2008)
Air entrainment, foaming of hydraulic fluids
How to control aeration (short video)
Cavitation or aeration? How to tell the difference (2017)
Foaming keeps coming up for discussion
Entrained air in hydraulic oil
How to control oil aeration (short video, 2015)
Learn Oil Analysis - Microdieseling (2018)
Microdieseling and its effects on oil (2012)

Air contamination can cause a great deal of harm to hydraulic systems. Unfortunately, unless the machine is foaming, with oil spewing from the top of the reservoir, we sometimes overlook this potentially devastating contaminant. Here are a few ways in which air contamination can undermine your reliability effort:

Spongy hydraulics - Air is compressible. This loss of control can slow throughput, increase the percent defective rate, and, in some cases, cause injury or death.

Gaseous cavitation - Some references say gaseous cavitation causes wear, others say it just makes noise. Play it safe and keep as much air out of the oil as possible.

Oxidation - The rate of oxidation is affected by a number of factors, but all else held equal, it is proportional to the amount of oil in boundary contact with air (which, of course provides the oxygen).

Thermal degradation - Did you know that compressing an air bubble from ambient pressure to 3,000 psi increases the bubble's temperature to more than 2,000 degrees F? This is hot enough to thermally degrade oil at the boundary contact between the air and the bubble, which darkens the oil, sometimes giving it a sooty appearance causing varnish to build up on component surfaces.

So, watch for signs of air entrainment or foaming, and take occurrences seriously. Also, periodically test your oil's ability to release air and its tendency to maintain stable foam. If you have recurring problems, evaluate the lube specification and the tank design, and check for low levels and signs of a suction line leak.
Drew Troyer, Noria
Air is both a normal ingredient, and a contaminant, of hydraulic oil. It's a normal ingredient because hydraulic fluid typically contains between 6 and 12 percent by volume of dissolved air. There's no avoiding this. And provided this dissolved air stays dissolved, it poses no problem to the hydraulic system or the fluid.
But if this dissolved air comes out of solution or air is ingressed, via the pump intake for example, the result is entrained air. These air bubbles are typically less than 1-millimeter in diameter.
Entrained air increases noise levels and decreases the efficiency of the system by reducing bulk modulus (fluid stiffness). And when entrained air bubbles are compressed at the pump outlet, extremely high peak temperatures result.
This compression of entrained air is said to be adiabatic. That is without transfer of heat to the surrounding fluid. However, localized heating of the oil film in contact with the air bubbles results in high-temperature 'cracking'. The result is oxidation and nitration which accelerate degradation of the fluid.
If that's not bad enough, these rapidly imploding air (gas) bubbles hammer the pump's valve plate and other critical surfaces resulting in erosive wear, a.k.a. cavitation erosion.
Prevention is really the only cure. Certain conditions cause dissolved air to come out of solution. When hydraulic oil temperature increases or static pressure decreases, air solubility is reduced and bubbles can form within the fluid. This release of dissolved air is known as gaseous cavitation.
Decrease in static pressure and subsequent gaseous cavitation often occurs at the pump inlet, as a result of:
--Clogged inlet filters or suction strainers.
--Turbulence caused by intake-line isolation valves.
--Poorly designed inlet (diameter too small, length excessive, multiple bends).
--Collapsed or otherwise restricted intake line.
--Excessive lift (vertical distance between pump intake and minimum fluid level).
--Clogged or undersized reservoir breather.

Air entrainment can also occur through external ingestion. Like gaseous cavitation, this commonly occurs at the pump as a result of:
--Loose intake-line clamps or fittings.
--Porous intake lines.
--Low reservoir oil level.
--Faulty pump shaft seal.

Air can be present in four forms:

- Free air - such as a pocket of air trapped in part of a system.
- Dissolved air - hydraulic fluid contains between 6 & 12 percent by volume of dissolved air.
- Entrained air - air bubbles typically less than 1 mm in diameter dispersed in the fluid.
- Foam - air bubbles typically greater than 1 mm in diameter which congregate on the surface of the fluid.

Of these four forms, entrained air is the most problematic.

Pre-filling components and proper bleeding of the hydraulic system during start-up will largely eliminate free air.

Small amounts of foam are cosmetic and do not pose a problem. However, if large volumes of foam are present, sufficient to cause the reservoir to overflow for example, this can be a symptom of a more serious air contamination and/or fluid degradation problem.

Negative effects of entrained air include:

- Reduced bulk modulus, resulting in spongy operation and poor control system response.
- Increased heat-load.
- Reduced thermal conductivity.
- Fluid deterioration.
- Reduced fluid viscosity, which leaves critical surfaces vulnerable to wear.
- Cavitation erosion.
- Increased noise levels.
- Decreased efficiency.

Certain conditions can cause this dissolved air to come out of solution, resulting in entrained air.
When fluid temperature increases or static pressure decreases, air solubility is reduced and bubbles can form within the fluid. This release of dissolved air is known as gaseous cavitation.

Decrease in static pressure and subsequent release of dissolved air can occur at the pump inlet, as a result of:

- Clogged inlet filters or suction strainers.
- Turbulence caused by intake-line isolation valves.
- Poorly designed inlet.
- Collapsed or otherwise restricted intake line.
- Excessive lift.
- Clogged or undersized reservoir breather.

Air entrainment can also occur through external ingestion. Like gaseous cavitation, this commonly occurs at the pump - as a result of:

- Loose intake-line clamps or fittings.
- Porous intake lines.
- Low reservoir fluid level.
- Faulty pump shaft seal.

Brendan Casey

Return pipes into hydraulic reservoirs should be larger than the intake pipes and should end below the surface of the oil in the reservoir. Locate the return as far away from the suction as possible to allow the oil as much residence time as possible. Better still, install a baffle between the suction and discharge. Cut the return pipe at an angle so that it directs the flow toward the tank wall.

1.9 Base stocks, saturates, aromatic hydrocarbons, API groups

Dr. Nancy McGuire - Fundamentals of base oils (2019)
Automotive base oil presentation
Chapter in a book: The evolution of base oil technology
Chapter in a book: Base stocks
Base oils
Classification of lubricants
Understanding base oils (2017)
Understanding the differences in base oil groups
The fundamentals of mineral base oil refining (2012)
Group II base oils spreading (2017)
Orbichem - Group I, II and III specifications (example)
Chevron Group II base oils
Chevron Group II base oils for industrial oils
ExxonMobil base stocks
Consider base oil and refining method when selecting lubricants
GTL: Gas to liquids refining
GTL: Gas to liquids produces extremely pure base oils
Re-refining: Bringing used oil back to life
Chinese re-refining process (2017)
Arslan Enginery - Used oil recycling plant
The evolving global bright stock market (2018)
Ergon - Bright stock alternative (VI = 81, 65% paraffinic)
Chinese plant makes Group III+ Bright Stock (21 June 2019)
Biodegradable lubricants (links)

Many of the benefits of high saturates Group II were discovered in use rather than being predicted, such as their much superior dispersant additive response in heavy-duty diesel applications.

1.9.1 What does 'synthetic' mean?

Oil base stocks (Mobil vs. Castrol on page 8)
What is a true 'fully synthetic' oil?

Synthetics - general

Petroleum-based mineral oils function very well as lubricants in 90 percent of industrial applications. However, they also have limitations depending on the type of base stock and additives used, the refining technology, and the operating conditions.

Conventional vs synthetic oil (short article, 2011)
Basics of synthetic oil technology
ExxonMobil synthetics (2015)
Chemours' Krytox - Perflouropolyethers (2017)
Benefits of perflouropolyethers
BASF - Hybrid high viscosity base stock
Methacrylates in combination with Group III in gear oils
Dow Corning - silicones (2017)
Molykote inudstrial lubricants (2007)
Molykote G-900X Series greases for high temperature applications (2017)

The formerly known manufacturer of Molykote lubricants has been Dow Corning, a joint venture between Dow Chemical and Corning Incorporated for over 73 years. In 2016 our parent company Dow Chemical took us over and last year we had a merger with Dupont.
Mathias Sottong

Silicone synthetic lubricants are used when resistance to oxidation, heat and/or water is important and the performance of other types of lubricants is unacceptable. Applications include high-temperature grease and the lubrication of oxygen compressors. Negatives for using silicone synthetics include high cost, poor boundary lubrication and poor additive solvency (they don't accept extreme-pressure and anti-wear additives).

Synthetics - usage

Daniel Rader - Synthetic oil or mineral oil? How to make the right choice (2021)
Seal considerations relevant when switching to synthetics
Mary Beckman - Squeezing energy from synthetics (January 2019)

The estimated improvements for the overall energy savings from a friction perspective only between Group III and PAO are in the range of 0.7% to 1.4%.

SAIT - Financial benefits of synthetic lubricating fluids (2016)
AAA report lauds synthetic oils
AAA report (2017, informative)
How true are the performance claims of synthetic engine oils? (2017)
Basics: When to use a synthetic gear oil (short, 2018)
Guidelines for selecting high-temperature lubricants
Synthetic gear oils
Choosing between synthetic lubricants and conventional oils
Advantages of synthetic base oils (2018)
Is synthetic motor oil better for your car? (7 minute video - Answer: Yes)
When does synthetic oil make sense? (short video)
Is synthetic oil better?
Are synthetic lubricants really that good?
PAO-based lubes make machines run cooler (2017)
Are synthetic lubricants always a wise choice?
KEW Engineering - Mineral or synthetic? - Scroll down
Selecting oils with high pressure-viscosity coefficient and increase bearing life
LE - When do synthetic lubricants make sense?
Synthetic lubricants for automotive components
Micro-pitting, wind turbines and using synthetics in gears (links)

Synthetic oils have better resistance to ageing and a longer service life, the time between oil changes could be three to five times that of mineral oils. Synthetic oils have improved thermal and oxidation resistance, improved viscosity/temperature characteristics, better low temperature properties and lower evaporation properties. In some instances, synthetic oils have less tendency to form residues.

1.9.2 Polyalphaolefins (PAO)

PAOs have inherently higher specific heats, so it will absorb more heat allowing the PAO-based lubes and the parts that they lubricate to run cooler.

Jeanna Van Rensselar - The bright future for PAOs (February 2021)
ExxonMobil - Group IV Basestocks: Polyalphaolefins (PAO)
AMSOIL - All synthetics are not created equal
Dodecene-based Synfluid PAOs
Synfluid mPAOs
Mobil 1: True PAO-based synthetic oil
Mobil SHC industrial lubricants (video)
ExxonMobil synthetic fluids and lubricant base stocks
ExxonMobil - Group IV base stocks: PAO
Mobilgear SHC XMP 320 in wind turbines

One property that can improve a machine’s efficiency and lessen energy and fuel consumption is known as the traction coefficient. Consider that if you are able to decrease the amount of force required to move a load across a lubricant film, you can reduce the amount of fuel consumed and the number of emissions produced. The traction coefficient is simply the amount of force required to move a load divided by the load. The closer this ratio is to 1, the more force is required to move the load. As the ratio decreases, less force is needed to move the same load.

Mineral oils by nature have millions of combinations of molecular shapes and sizes in each drop. This inconsistency in molecular size results in a higher traction coefficient. Synthetic base oils are manmade compounds and have much more consistency in several key areas, including their fluid properties and molecular size. This allows a load to move more easily across the lubricant film, thus lessening energy consumption and emissions.

To envision how this works, imagine pushing a sheet of plywood across a series of balls. If the balls are different shapes and sizes (footballs, basketballs, baseballs, etc.), moving the piece of plywood becomes more cumbersome and awkward. Now if you took that same sheet of plywood and pushed it across a series of tennis balls, with each ball the same shape and size, it becomes much easier. This is why most synthetic oils come with claims of reducing energy consumption and can actually help to decrease emissions.

Food-grade lubricants

(Beyond the scope of the book)

Dr. Nancy McGuire - Incidental contact lubricants for the food industry (2019)
Food-grade lubricants
Advantages of food-grade lubricants (2012)
NSF certified 'food-grade' lubricants
MOSH and MOAH dangerous?
ELGI - The selection and usage of food safe lubricants
Lubriplate - The continuing evolution of food grade lubricants
Lubriplate - H-1/Food grade lubricants
PAG food-grade lubricants
SKF introduces food-grade lubricants
Evonik - Viscoplex 8-219 VI improver for hydraulic fluids registered by InS Services as HX-1 ingredient for H1 lubricants with incidental food contact

The United States Department of Agriculture (USDA) created the original food-grade designations H1, H2 and H3.
H1 lubricants are food-grade lubricants used in food-processing environments where there is the possibility of incidental food contact.
H2 lubricants are food-grade lubricants used on equipment and machine parts in locations where there is no possibility of contact.
H3 lubricants are food-grade lubricants, typically edible oils, used to prevent rust on hooks, trolleys and similar equipment.
R. Auerswald

1.9.3 Other synthetic hydrocarbons

Alkyl benzene as a compressor lubricant
Alkylated naphthalenes
King Industries - Alkylated naphthalenes (2017)
Anuj Kumar - Polyisobutylene market (2019)
Polyisobutylene
TPC Group - Polyisobutylene
BASF - Polyisobutylene

1.9.5 Polyalkylene glycols (PAG) (polar compounds)

PAG synthetic oil
Polyalkylene glycols
Polyglycols for lubricating large gear drives
Friction and wear reduction mechanism of polyalkylene glycol-based engine oils (2018)
Polyalkylene glycol - synthetic turbine fluid technology
Turbine lubricants: biodegradable, preventative alternatives
Synthetic gear oil selection - See wear of aluminium components
New synthetic OSPs for high performance greases
Klüber: Changeover from mineral oil/polyalphaolefin to polyalkylene glycol
Ucon OSP - oil soluble PAG
Oil soluble synthetic polyalkylene glycols
Innovations in PAG based lubricants
Energy efficient industrial gear lubricants
Sullube - Laboratory analysis of PAG in service
Heat of combustion, flash point, autoignition temperature of PAG
Effects of water on PAG
Removing water from PAG
Worm gears (links)

Sludge and varnish in hydraulic controls of turbines is not a problem with PAG turbine oils owing to their high solubility. However, some PAG turbine oils cause sudden oxidative degradation, resulting from a decrease in anti-oxidants due to poor thermal stability of those PAG base oils.

1.9.6 Esters, amides, environmentally friendly lubes

Rapeseed natural ester fluid for Extra High Voltage transformer (2020)
Cargill natural ester fluid for South African electrical grid (2020)
Schaefer - Esters in synthetic lubricants
Schaefer - Esters in synthetic lubricants
Synthetic esters
Inolex - White papers on esters
Wikipedia - Polyol esters
Rexroth - List of environmentally acceptable hydraulic fluids
Croda Lubricants to launch new Group V base oil technology (amides)
Emery Biolubricants (Esters)
Environmentally friendly lubes for marine use (2017)
Erlend Hanssen Nervold - Ensuring satisfactory aft stern tube bearing lubrication performance (3.1 Mb, 2019)
Erlend Hanssen Nervold - Natural ester oil application in liquid filled transformers (3.3 Mb, 2019)

Vegetable oils and biodegradable lubricants

(Beyond the scope of the book)

Jeanna Van Rensselar - Biobased base stock (2021)
Erik Willett - Water-soluble thickeners for industrial and ecofriendly lubrication (2020)
Are biobased lubricants food for microbes? (2018)
Biodegradable lubricants (2012)
Improving vegetable oil properties for lubrication
Biodegradable oils - How to apply and maintain
Controlling degradation in biodegradable greases
New test methods for lubricant biodegradability
Proposed ASTM biodegradable hydraulic fluid standard
Vincent Bouillon, BfB Labs - Assessment and verification of environmental acceptable hydraulic fluids (EAHF) according to the European Ecolabel’s revision, Part 2 (2019)
What you should know about environmentally friendly lubricants

1.9.7 Naphthenics

Nynas - Base oil handbook
Nynas - Group I replacement with naphthenics
Nynas - Naphthenic oils for greater efficiency
Nynas - Anti-oxidant response of low sulphur naphthenic base oils (2017)

1.10 Oil performance, performance additives

Additives in lubricating oils
The chemistry and function of lubricant additives (2017)
Dr Robert M. Gresham - The mysterious world of lubricant additives (2012)
The contributions of additives
Lubrizol - Lubricant fundamentals 2: additives (video, introduction in end Part 1)
Formulations of lubricating oils
Additives
Lubricant additives
Noria - A practical guide to lubricant additives (comprehensive, 2018)
Dr. Neil Canter - Sulphurized additives: Types available, key applications and beneficial properties (2019)
Infineum - Additives (2017)
The truth about additive depletion (video)
The critical role of additives in lubrication (2012)
How to determine the quality of a lubricant additive
Dr. Robert M. Gresham - Detergents and dispersants (2018)
Rhein Chemie additives
ZDDP (links)

Neither mineral nor synthetic base oils can satisfy today’s lubricant performance requirements without using additives. Additives are chemical substances, in most part synthetic, which are used in lubricant formulations to adjust a broad of spectrum of properties by enhancing what is desired and suppressing what is unwanted. Many additives are multifunctional products that may exhibit synergistic or antagonistic behavior when mixed together. As a rule of thumb, additives do not add. This makes balancing and optimization of additive systems a challenging task.

1.11 Water separability (demulsibility)

Hi-Pro - Getting to know demulsibility (2021)
Jennifer Yeadon - Steam turbines and the battle for good demulsibility (2019)
Hi-Pro - Demulsibility (video, 2019)
The importance of demulsibility in oil
TESTOIL - Demulsibility
Water separability
Test Method for Water Separability
Demulsibility ASTM D 2711

1.12 Supplemental ('proprietary') additives

Pros and cons of enhancing your oil with additives (short, 2019)
Advice for improving oil with additives (2012)
The disadvantages of using anti-friction metal conditioners
The advantages of lubricant conditioners
How engine cleaners affect your oil

Blue exhaust smoke indicates an engine is headed for serious mechanical failure due to a high oil ingress into a combustion chamber. This means an engine is burning too much oil due to worn intake valve guides or poor piston ring control – collapsed or worn rings.
A useful rough guide to measuring oil consumption is the ratio of oil consumption to fuel consumption, because the harder an engine works (fuel consumption) the more oil it will use. A good estimate is 0,6% of total fuel consumption.

REVISION 1

Answers to REVISION 1 (link)

3.1 Engine oils, engine oil additives, ZDDP, fuel economy

Dr Raj Shah, Dr Mathias Woydt, Isaac Kim - Maximizing fuel economy by thinning lubricating oils (2020)
Engine oil specifications
What is the best oil for my car (2018)
Dr. Nancy McGuire - The drive for efficient performance (2018)
Engine oil quality (2015)
Spectro Scientific - Webinar: Engines 101, Understanding basic engine operation
Engine oils
Lubrication system: Engine oil functions (video)
Low speed pre-ignition (2019)
Selecting the correct lubricant
Wikipedia - Motor oil
AMSOIL - European motor oils and SAPS content (2018)
Michael C. Brown - Engine oil differences (2016)
Dr. Robert M. Gresham - Detergents and dispersants (2018)
Peter Wright, INFINEUM - The art of dispersant design (2018)
Friction, lubricants, energy losses, tribo tests, engine oils, base oils, additives, coatings
Passenger car engine oil change intervals: past, present and future (2018)
Additives boost fuel economy
Friction and wear reduction mechanism of polyalkylene glycol-based engine oils (2018)
Dr. Neil Canter - ZDDP's uncertain future (2019)
The anti-wear additive zinc dialkyldithiophosphate
Certain amount of ash in the lubricant is needed to increase the filtration efficiency of the gasoline particulate filter (2019)
Elco ZDDPs
Zinc phosphate reaction with iron oxide
Joanna Dawczyk et al. - Film thickness and friction of ZDDP tribofilms (scientific paper, 2019)Joanna Dawczyk
History of ZDDP
BASF - IRGALUBE FE1 - Save fuel by interacting with ZDDP (2017)
Dr Wilfred T. Tysoe and Dr Nicholas D. Spencer - ZnDTP alone as a primary suspect in the formation of white etching cracks (2019)
Toyota - Better antioxidants, higher quality base oils to prevent turbocharger coking
New low viscosity grade engine oil specifications in Japan
Antifreeze contamination in motor oil (short video)

There are many different quality oils on the market.
At the starting level, we have many brands sold by the dollar stores and convenience markets that are very basic, cheap base oil with minimal, cheap additives. They may or may not pass the API tests, and probably are not registered (so don’t have the Donut and starburst.
Then you have four levels. Look for a moment at big brands. Castrol (as an example) has an entre level GTX that meets the minimum API standards when new and for the minimum time for certification. Then they have Magnatec, which is a much better blend of base oils and a better package of additives. They also have two different synthetic oils, one for price point, made with Group III base oil, and one with traditional PAO synthetic base oil.
Most of the big brands do something along the same lines. I used to carry only the second and fourth (a great semi-synthetic, similar to the Magnatec, and a great PAO/Ester synthetic, similar to Mobil1). About 2 years ago, I started to add the 3rd level (group III synthetic) for people who insisted on synthetic but would go to Castrol for the cheaper product. I am phasing this one out, as once people try the real PAO synthetic, they are not satisfied with the cheaper version.
Richard Widman

ZDDP reaction films formed on rubbing contacts produce enhanced friction in mixed lubrication conditions. The ZDDP reaction film appears to inhibit lubricant entrainment into the contact, thereby leading to a reduced EHD film thickness compared to ZDDP-free lubricants.

Turbocharged gasoline direct injection (TGDI) engines suffer from the presence of particulates in vehicle exhaust emissions, similar to a diesel engine. New oil specifications are needed to counter that.

Friction and wear

(Beyond the scope of the book)

John Cummins - Failure mode and effects analysis (2016)
tribonet - Friction (2016)
Wikipedia - Friction
Castrol - Friction Reducing Technologies – Fact or 'Friction'
Friction and traction
Rolling friction
Friction theory
tribonet - Droplet friction is similar to solid friction (2017)
How to reduce friction between surfaces
Friction modifiers
Friction modifiers (2015)
Superlubricity (2017)
Tribological design guide part 5: Wear theory
Wear theory
Learn Oil Analysis - What is the difference between normal and abnormal wear (2019)
Researchers simulate wear of materials as they rub together (2016)
Basics of wear
Polishing wear (2018)
Fretting wear (2021)
Wear = the silent killer
Randy Riddell - The keys to solving fatigue, the silent killer (2019)
Premature wear (short)
Three common contaminants and the oil analysis tests that can detect them
Nanopolishing for surface perfection
Basic wear modes in lubricated systems
Common causes of machine failures
Types of engine bearing damage
Main bearing failure chart
Bore glazing and polishing in diesel engines

Friction modifiers are most efficient under boundary conditions or where metal-to-metal contact occurs. Organic friction modifiers have long, soluble chains and a polar head. The polar head attaches to the metal surfaces. The soluble chains line up beside each other much like fibers in a carpet. The polar heads may be comprised of phosphoric or phosphonic acids, amines, amides or carboxylic acids. The soluble chains form dense mono layers or thick, reacted viscous layers. These layers shear easily and create a relatively slippery surface.

Corrosive wear occurs when a machine surface is damaged by chemical attack. The responsible corrosive chemical could be either vaporous or liquid, which might be found in a plant that mixes or handles strong acid or alkali materials. Often the damage to lubricated surfaces comes from acidic by-products generated by the deterioration of the lubricant.

Using composites with a metal matrix and graphite particles takes advantage of self-organization to provide solid lubrication, says materials scientist Pradeep Rohatgi at the University of Wisconsin-Milwaukee. For example, a bearing made out of copper or aluminum contains particles of graphite embedded in the surface. As the surface of the bearing wears down, the graphite smears, forming a film of graphite. The exceedingly low coefficient of friction corresponds to graphite, not the metal the tribofilm is sandwiched between.
Mica, talc and molybdenum disulphide also are possible solid lubricants, but graphite is the most popular because it is the cheapest and has the lowest friction coefficient.
Calcium is a commonly used dispersant in oil due to its low cost and high availability, used to keep any debris collected by the oil from forming a sludge. However, when calcium mixes with the soot calcium phosphate forms, resulting in abrasive particles of soot. This abrasiveness rubs against the engine parts, causing wear and deterioration in effectiveness.
Dr Pranesh Aswath

Sludge, drain intervals, maintenance

(Beyond the scope of the book)

Engine oil sludge
Learn Oil Analysis - What happens in engine oil to cause sludge (2018)
Combating and removing engine oil sludge
Evan Zabawski - The 3000-mile myth (2019)
Optimizing oil change intervals in heavy-duty vehicles
Extending oil change intervals on heavy mining equipment
Extending preventive maintenance (PM) intervals
Used-oil analysis for predictive maintenance
Why predictive maintenance does not work
Proactive and predictive maintenance (links)
Cepsa - FAQ
FAQ after Noria webinar How to detect and control lubrication failure modes

Fresh engine oil (before it gets into the engine) normally has a cleanliness level in the range 16/xx to 18/xx. As soon as it gets into the engine, the cleanliness drops one-two levels because of mixing with the remaining old oil. An oil is "dirty" when cleanliness drops to 21/xx to 23/xx.
Prof. Dr Boris Zhmud

3.2 Engine oil specifications, API service categories

Engine oil licensing and certification system (June 2019)
API updates Motor Oil Guides, to license new passenger car engine oil category sometime in 2020 (2018)
Oil matters guide (June 2018)
API Lubricants Group approves provisional licensing (30 June 2017)
Infineum - North American specification update (14 June 2017) Heavy duty tests scrutinized (2017)
Infineum - API Engine Oil Classifications (2017)
Engine oil specifications: Is the system broken?
API Engine Oil Service Categories
API Engine Oil Classifications
API Service Classifications
API licensing documents
API - Engine oil licensing
API - Engine oil licensing
API - Engine oil guide
API SN and SN-RC performance specifications
API Licenses
API pulls plug on ‘Energy Conserving’
API to discontinue licensing of 'Energy Conserving' oils for API SL and SM
New motor oils are bad for older engines (scroll down)
API base oil interchangeability
API guidelines for SAE viscosity grade engine testing
API certification system, 17th edition, Sept. 2012, 136 pages
The Sequence VIII test run on engine CLR L-38 ran out of bearings
Comparing gasoline and diesel engine oils

The lubricant in a crankcase engine is subjected to very complex conditions, with many different conditions in different parts of the engine, variable patterns of driving behavior, and, critically, the contamination of the lubricant by reactive combustion gases and particulates. This makes it very difficult to relate engine/lubricant performance to simple bench tests, and a key feature of engine oil development and testing is the use of engine tests to assess the behavior of the lubricant in the complex combination of conditions present in a firing engine.
Automotive Lubricants and Testing

Valvoline advertised that their oil is better than Mobil 1. I asked in Quora what did ExxonMobil say to that. Bradley Cosgrove replied:
ExxonMobil complained to the API, American Petroleum Institute, the oil trade association, and the API told Valvoline to stop. The results of the sequence tests are not supposed to be used for marketing.
In fact, Valvoline's claim is not a big deal. The sequence IVA is not the hardest test to pass. And it was replaced with the IVB for GF-6.
Oil formulators mainly focus on the IIIG, oxidation, and VIE, or VIF based on the viscosity grade, fuel economy, and VH, sludge.
If they can pass those tests, they can pretty much pass the other two, IVB and VII.
I would be interested to know if Valvoline’s advertised IVA oil was the final formulation, or just a test blend. The oil companies can change formulations slightly when running each test and the final formulation would be something of a combination of the different formulations. The final formulation would pass IVA, but maybe not as well as the formulation that was run to achieve the best IVA.

3.2 API service categories - diesel engine oils

API - Latest oil categories (2016)
API CK-4 and FA-4 is done
API approves CK-4 and FA-4 Diesel Engine Oil Categories
Chevron - API CK-4 and FA-4 explained
Shell - API CK-4 and FA-4 (promotional video)
Shell unveils CK-4, FA-4 strategy
Shell - Mobil Delvac 1300 Super 15W-40 does not meet API CK-4 nor Volvo, MACK and Cummins (2018)
ExxonMobil responds to Shell's claim that Mobil Delvac 1300 Super is not meeting API CK-4 (25 June 2018)
ExxonMobil's reply
Ford issues list of acceptable DEOs
Ford issues list of acceptable DEOs (2018)
Ford recommends FA-4 for F-150 (August 2018)

Paccar does not allow use of API FA-4 oils in any of its MX or PX engines.

By the end of March 2019, API has only licensed 100 FA-4 products.

Trucks are able to get 1 to 2 percent better fuel economy using FA-4 oils.

API CK-4 and FA-4 licensed manufacturers (December 2016)
Cummins' CES 20086 and CES 20087 registered oils
Cummins' CES 20086 registered oils
Cummins' CES 20087 registered oils
Detroit Diesel - approved API CK-4 oils
Detroit Diesel - approved FA-4 oils
API CJ-4 performance specifications
Proposed ASTM standard to evaluate diesel engine oils in T-13 engines (2016)
The background behind diesel particulate filters (DPF, 2018)

API Service Category CK-4 describes oils for use in high-speed four-stroke diesel engines designed to meet 2017 model year on-highway and Tier 4 non-road exhaust emission standards as well as for previous model year diesel engines. These oils are formulated for use in all applications with diesel fuels ranging in sulphur content up to 500 ppm (0.05% by weight). However, the use of these oils with greater than 15 ppm (0.0015% by weight) sulphur fuel may impact exhaust after-treatment system durability and/or oil drain interval.
API CK-4 oils exceed the performance criteria of API CJ-4, CI-4 PLUS, CI-4, and CH-4 and can effectively lubricate engines calling for those API Service Categories - they are backward compatible.
API Service Category FA-4 describes certain XW-30 oils formulated for use in high-speed four-stroke diesel engines designed to meet 2017 model year on-highway and Tier 4 non-road exhaust emission standards with diesel fuel sulphur content up to 15 ppm (0.0015% by weight). Refer to individual engine manufacturer recommendations regarding suitability of API FA-4 oils.
API FA-4 oils are not interchangeable or backward compatible with API CK-4, CJ-4, CI-4 PLUS, CI-4, and CH-4 oils.
With the introduction of API CK-4 and API FA-4 diesel engine categories, Cummins developed two new standards, CES 20086 and CES 20087. Cummins has updated its CES 20086 list of API CK-4 registered oils, Cummins CES 20087 lists API FA-4 registered oils.

3.3 and 3.4 Sulphated ash, TBN

Prof. Dr Boris Zhmud - TBN (LUBE Magazine April 2018)
Low SAPS / low ash
TBN, oxidation and additives
Why an oil's base number (TBN) drops
Engine oils' BN (base number) and i-pH value
Learn Oil Analysis - What do TAN and TBN mean (2018)
Measuring reserve alkalinity
Spectro - Measuring TAN and TBN

3.5 ILSAC (International Lubricant Standardization and Approval Committee)

Infineum - ILSAC GF-6 engine tests (2020)
Infineum - ILSAC GF-6 menu
ILSAC GF-6 major milestone: yes vote for proposed limits (2019)/a>
Automakers ask API to update GF-5 now (26 July 2017)
Engine oil specifications: Is the system broken?
ILSAC GF-5 official
GF-5 performance requirements
Toyota Valve Train Wear Test ready for precision matrix testing
Lubrizol - Future ILSAC_GF-6 web site
Infineum - ILSAC_GF-6 web site
Lubrizol additive for SAE 0W-16

The Lubrizol Corporation announced that Lubrizol PV1510 engine oil additive technology, designed to meet the complex requirements of the ILSAC GF-6 specification, is ready (April 2019)

3.6 ACEA (Association des Constructeurs Européens d'Automobiles) and Equipment Manufacturers (OEM)

ATIEL seeks to forge closer working relationship with API (2019)
Nick Augusteijn - ACEA 2018 delayed until 2020 (2019)
ACEA specification update (11 April 2018)
Europe base stocks and formulations (2018)
ACEA European oil sequences 2016
Infineum - ACEA 2016 brochure
AlterEvo Ltd blog 31.1.17 - ACEA 2016 Sequences
ACEA European oil sequences 2012
Lubrizol - ACEA European Oil Sequences 2012
Sarma - ACEA 2012 versus ACEA 2010 detailed comparison
European passenger car specifications
The ATIEL Code of Practice
ACEA Sequences: Combined claims guidance
Lubrizol - Relative performance tool
ACEA 2016 boosts oil performance
ACEA European oil sequences 2016
Infineum additives meet ACEA C5-16 requirements

In the M111 fuel economy test, ACEA C5-16 has a requirement set at 3.0% which is 0.5% higher than C2-16 at 2.5% and significantly higher than C3-16 at 1.0%.

ACEA E6-16 oils are low SAPS, Ultra High-Performance Diesel (UHPD) lubricants designed for use in severe duty, long drain applications. ACEA E6-16 is usually coupled with Daimler MB-Approval 228.51 and MAN 3677, MTU oil category 3.1 and Deutz DQC IV-10 LA.
Typically, Daimler, MAN, MTU and Deutz performance specifications build on top of an ACEA E6-16 with additional performance requirements in areas such as wear protection.

3.9 Two-stroke petrol engines

Wikipedia - Two-stroke engine
Wikipedia - Two-stroke oil
Wikipedia - API TC
Wikipedia - JASO M345 standard
Dan's Motorcycle Repair Course - Two-stroke oil
Can using two stroke oil in a four stroke engine affect it?

3.10 Outboard motor oils

NMMA - TC-W3 Two-stroke oil certification program
Do I need TC-W3 engine oil?
NMMA issues its 2018 TC-W3, FC-W, and Catalyst Compatible FC-W certified oils lists
Understanding two-stroke engine oil

3.11 Motorcycle oils

Lubrizol - New demands for motorbike oils (2020)
INFINEUM - Next generation motorcycle oils (2018)
Lubrizol - Motorcycle oils
Lubrizol - Efficient motorcycle oils (presentation, 2019)
Jaso oil specifications
New JASO T 903:2016 replaces the 2011 version for high friction (MA/MA1) and low friction (MB) oils
Jaso MA and Jaso MB classifications
Lubrizol - Jaso MA and MB
Lubrizol - Differences between Jaso MA and MB
What does Jaso MA2 mean? (Scroll down to discussion)
API SL and API SM formulations contradict Jaso-MA/MA1/MA2
Jaso updates four-stroke motorcycle specification
Lubrizol - Two-stroke motorcycle oils - Jaso M345 standard
Wikipedia - Jaso M345 standard
Motorcycles: Synthetic versus mineral oils
Motorcycle lubricant specifications lacking - Go to page 6
How to change your motorcycle oil (video)
Kawasaki launches motorcycle oils in Malaysia (2018)

Ducati calls for the chain to be cleaned and lubed every 1000 km. Also adjust your chain. Every time you clean, check the slack and adjust as needed.

Electric vehicles

Dr Edward P. Becker - Gear lubricants in electric vehicles (2021)
Electric vehicles lubricant technology (2019)
tribonet - Tribology and electric vehicles (2019)
Jane Marie Andrew - The future of lubricating greases in the electric vehicle era (May 2019)
Hans van de Groenendaal, South Africa - Charging electric cars is not without its challenges (15 February 2019)
Dr. Edward P. Becker - Lubrication and electric vehicles (February 2019)
Jeanna Van Rensselar - Electric vehicles (2019)
Total launches fluids for electric and hybrid vehicles (6 December 2018)
Minimal impact of vehicle electrification seen on lubricating greases (11 October 2018)
Lubrication electric vehicles (LnG EMEA October 2018)
Lubrication challenges of hybrid and electric vehicles (2018)
Ricardo - Balanced use of technologies is preferable to sole focus on electrification (3 October 2018)

70 percent of new passenger cars sold in 2030 will still have internal combustion engines.
The peak of ICE vehicle production is not expected until 2024, after which time the share of BEVs is projected to grow to 15 percent in 2030. By that time, though, the vast majority of the global fleet of cars–92 percent–is still expected to consist of ICE vehicles.
Schlegel und Partner, 2019

3.12 Gas engines

Peter Harteveld - Gas engine oil for biogas applications (2021)
Deposits of silica or silicates from biogas can adhere to the cylinder heads and pistons causing problems (2020)
Petro-Canada Lubricants launches new and improved DURON GEO (2019)
Infineum Insight - Multifuel lubricant technology (2019)
Functions of oils in gas engines
Generation using gas-fuelled engines
Lubricating natural gas engines
Natural gas engine lubrication and oil analysis
Causes of nitration in engine oil
Gas engine oil analysis: what does the TAN/TBN crossover really mean?
Learn Oil Analysis - What do TAN and TBN mean (2018)
Cummins issues new NGEO specification CES 20092 (2018)/a>

3.13 Marine engines and emergency power generation, marine lubes

Marine diesel engines
The Wärtsilä RT-flex96C, the world’s largest and most powerful diesel engine in the world today. Built in Finland, the RT-flex96C’s fourteen cylinders can deliver 80080 KW of power or enough to power an entire suburban town. The engine weighs 2,300 tons, stands 44-feet tall and is 90-feet long. In 2006, the Wärtsilä RT-flex96C engine was installed and finally set sail on the Emma Mærsk, a cargo ship that can carry 11,000 20-foot shipping containers at a breakneck speed of 31 knots.
Total Lubmarine launches Talusia Optima cylinder lube
Environmentally friendly lubes for marine use (2017)
Group II base oils in trunk piston engines (2017)
Marine engine cylinder oils (2017)
Chevron Marine Lubricants to phase in Taro Ultra oils in 2019
Croda launches range of non-sheening base fluids (2020)

British diesel locomotive engines use SAE 15W-40 engine oil in diesel locomotives for more than 30 years.

3.15 Gas turbines

Wikipedia - Gas turbines
AeroShell Turbine Oil 500
Mobil Jet Oil 387
Mobil Jet Oil 387 gets approvals from GE Aviation (2018)
Mobil Jet Oil 387 gets approvals for Rolls-Royce Trent 700, Trent 800, RB211-524 and RB211-535 engines (2016)
Mobil Jet Oil 387 gets approvals from Pratt & Whitney for TM 1500G engines (2017)
Mobil Jet Oil 387 gets approvals from Pratt & Whitney for PW1100G-JM and PW1400G-JM engines (2017)
Mobil Jet Oil 387 gains new approval with GP7200 engines (2017)

3.16 Automotive gear oils for manual gearboxes and final drives

Wikipedia - Gear oils
Widman - The difference between GL-4 and GL-5
Lubrizol - API GL-5
Manual transmission oils - is thinner really better?
A new level of performance: China GL-5 PLUS
ZF - Lists of lubricants
ZF has updated its lists of approved lubricants (2018)
Gear oil additive package Afton HiTEC 343
Magnetic plugs in dozer final drives
Used oil analysis determines the oil change interval in a big gearbox (2017)
Advances in manual transmission design and lubrication
How Haldex All Wheel Drive (AWD) works (video, 2017)

Q: What manual transmission oil does the 2019 Toyota Yaris take?
A: Toyota’s own 75W fluid, in reality is a synthetic SAE 75W-85 viscosity with the newer non-sulfur/phosphorous additive technology.
If you put thicker oil in it, or one with the sulfur/phos additives, you will ruin it.
Richard Widman

3.17 Limited slip differentials

Wikipedia - Limited slip differential
Castrol - Limited slip gear oil
Mobil - Limited slip gear oil
Doctoral theses: Wet clutch tribology - Friction characteristics in limited slip differentials

3.18 and 3.19 Eaton (form. Fuller) and ZF-FreedomLine, Caterpillar

Eaton Approved Lubricant Suppliers TCMT0020 EN-US, March 2015
Eaton revises its lubricant suppliers list (2018)
May 2018: Eaton lubricant suppliers list
Roadranger SAE 50 Synthetic Transmission Lubricant
Eaton - "Genuine Roadranger" and other lubricants
Cognis Emgard 2979 SAE 50
Cognis Emgard 2979 SAE 50
ZF-FreedomLine manual - select page 11
Caterpillar final drive and axle fluid requirements (2001)
Caterpillar revises its machine fluids recommendations bulletin (2017)
Caterpillar machine fluids recommendations (2017)
Barloworld - Caterpillar fluid specifications and recommendations

3.20 Allison

Allison transmissions - Click on Fluids
Allison fully automatic transmissions for road use
Allison vocational model guide
Allison oil analysis test recommendations

3.21 Total Acid Number (TAN)

Wikipedia - Total Acid Number
Learn Oil Analysis - What do TAN and TBN mean (2018)
Oelcheck - NN (neutralisation number) or AN (acid number)
Acid number tests
Parker Kittiwake - General information regarding AN

3.22 Automatic transmission fluids (ATF)

Gearboxes and transmissions
How torque converters work (video)
Wikipedia - Automatic transmission fluid
Facts about automatic transmission fluids
Types of automatic transmission fluids
ATFs today, from http://pqiamerica.com/ATFSURVEYFOLDER2017/PQIA_ ATF_ SURVEY_ REPORT_2017.pdf
ATF labels face a rewrite (26 July 2017)
Discussion: JASO-1A
Mobil's six automatic transmission fluids
Castrol automatic transmission fluids
Automatic transmission flushes (video)

3.23 Farm equipment oils, UTTO, STOU

Chevron Oronite launches innovative THF additive meeting new ZF spec (2020)
Transparency sought for tractor fluids (2018)/a>
Missouri retailers ordered to stop selling John Deere 303 (2017)
Maintain a tractor
How to keep your tractor running (book)
Lubrizol - Universal tractor transmission oils
Lubrizol - Universal Tractor Transmission Oil (UTTO) additives
Fuchs TITAN UTTO - Also click AGRIFARM UTTO MP on the left
Caltex Super Tractor

John Deere developed JD 303 in 1930 and replaced it 1974. Products making exclusive JD 303 claims can no longer be tested for compliance. JD 303 was replaced with J14-B, which was then replaced in 1978 with J20-A. John Deere has declared all of those specifications obsolete and has two current specs – JDM J20C and J20D (which are backward compatible) – along with its genuine Hy-Gard fluid. Some lubricant marketers had continued marketing hydraulic tractor fluids labelled as meeting the 303 standard but critics have said they do not meet the lubrication requirements of modern tractors and can harm them through effects such as damage to the spiral gear in the final drive and causing excessive wear in the planetaries.

September 2020: Oronite has achieved an important milestone by achieving one of the first approvals of a tractor hydraulic fluid (THF) additive offering that meets the new ZF TE-ML 05E specification.

3.24 Brake fluids

Wikipedia - Brake fluid

REVISION 2

Answers to REVISION 2 (link)

5. Lubrication conditions, EHL, anti-wear, EP

Lubrizol - Lubricant fundamentals 1 (video)
States of lubrication
tribonet - Hydrodynamic lubrication (2017)
Wikipedia - Hydrodynamic lubrication
Lubrication
Lubrication regimes
Elastohydrodynamic Lubrication (EHL) theory
Timken - The right thickness of lubricant
How temperature impacts oil condition
The effects of temperature on lubricants (2007)
EHL with greases
How lubricants combat friction and wear (2012)
Friction modifiers
Friction modifiers (2015)
Jeanna Van Rensselar - Extreme pressure and anti-wear additives (2018)
Wikipedia - Extreme pressure (EP) additives
Dr Neil Canter - Extreme pressure additives
The role of Extreme Pressure additives in gear oil
Dr Yulia Sosa - Extreme pressure and antiwear additives in rolling bearing lubrication (2021)
Limitations of EP additives
The effects of EP additives on worm gearboxes (2012)
The danger of EP additives on worm gearboxes (short video, 2018)
Elco extreme pressure additive
Jane Marie Andrew - Solid lubricants (2019)
Solid-film lubricants
Jane Marie Andrew - Expanding the repertoire of solid lubricant molybdenum disulphide (2021)
Wikipedia - Molybdenum disulphide
IMOA - Molybdenum sulphur compounds in lubrication
Climax Molybdenum - Molybdenum disulphide in lubricant applications
High temperature graphite bearing lubricant

At pressures above about 3000 psi (206 bar) there begins a significant increase in the viscosity of mineral oils. At 5000 psi (345 bar) the viscosity of a typical Group I base oil is approximately double its viscosity at atmospheric pressure. At higher pressures, the rate of viscosity increase accelerates and at very high pressures mineral oils cease to behave like liquids and tend to become waxy solids. Pressure viscosity coefficients are different for different types of oils, particularly for synthetic oils.

Metal sulfite, or Molybdenum disulfide (MoS2), is widely used as an additive in solid lubricants because of its low friction properties and robustness. However, at low loads or resistance, it shows excessive wear and higher friction.

A novel definition by Noria:
Film strength can be described as the lubricant’s ability to lessen the effects of friction and control wear by means other than the film thickness. As mentioned, the viscosity is the primary contributor to film thickness during hydrodynamic and elastohydrodynamic lubrication.
When the base oil viscosity is insufficient to overcome metal-to-metal surface contact, the base oil and additive chemistry work together to create a surface protection mechanism. During these boundary conditions, boundary lubrication is also influenced by the chemical and physical properties of the mechanical surfaces and any contributing environmental factors.
See the following article:

The importance of lubricant film strength (2017)
Film strength and load carrying capacity of lubricating oils (1958)

Using composites with a metal matrix and graphite particles takes advantage of self-organization to provide solid lubrication, says materials scientist Pradeep Rohatgi at the University of Wisconsin-Milwaukee. For example, a bearing made out of copper or aluminum contains particles of graphite embedded in the surface. As the surface of the bearing wears down, the graphite smears, forming a film of graphite. The exceedingly low coefficient of friction corresponds to graphite, not the metal the tribofilm is sandwiched between.
Mica, talc and molybdenum disulfide also are possible solid lubricants, but graphite is the most popular because it is the cheapest and has the lowest friction coefficient.

6. Industrial gear oils

Wikipedia - Gears
Industrial gear oils in 2016
Gear drive lubrication performance improvements (page 18, 2018)
Lubrication of gears
John Sander, LE - Selecting gear lubricants (pdf)
John Sander, LE - Selecting gear lubricants
Selecting the right industrial gear oil
Precision gear lubrication
Roymech - Gear lubrication
Trends in industrial gear oils (2008)
Formulation challenges for industrial gear lubricants (2018)
AMSOIL - DIN 51517 Part 3 (CLP) update (2010)
Klüber - Common industrial gear oil specifications (short)
Gear drive lubricants
Lubrication selection for enclosed gear drives
Trends in industrial gear oils
Maximising gearbox performance
FZG test description (Shell Tellus S)
LE - Improving gearbox lubrication by oil analysis condition monitoring, FZG machine
Gear lubrication - Gear protection also at low oil temperature
Troubleshooter’s guide to gear drives
Lubricant problem in an industrial gear drives (2019, includes two contributions by Petr Vavruch)
Changing bad gear oil habits (2016)
Monitoring large particles in gear oils
Flushing methods (Solving recurring oxidation problems)
Articles by Lawrence G. Ludwig
GEAR Solutions - Articles
Xtek - Technical papers - select gear terminology
SPX Cooling Technologies - Evolution of cooling tower gearboxes (2018)
Improving anti-rust property of EP industrial gear oil (sale offer)
Vavruch and de Vaal - New industrial gear oil: focus on EP performance
Impact of gear tooth surface roughness and advanced coatings on effective gear tooth friction coefficient (2017)
SEW-Eurodrive - Equivalents - Pages 185-6
ExxonMobil - Energy efficient industrial gear lubricants (2013)
Lubrizol - Developing an energy-efficient industrial gear oil (2017)
Shell Omala grades
TOTAL gear oils
Idemitsu TDF continuously variable transmission oil
Lubricating with FlexGear
Coupling lubrication and maintenance requirements (2002)
Couplings - Articles
Grease-filled gearboxes (links)

Overfilling a gearbox sump can be just as damaging as underfilling. Overfilling may cause air entrainment and foam, overheated oil, and leakage due to overflow. Over time, oxidation may also occur due to increased temperatures and exposure to air.

Micro-pitting, wind turbines and using synthetics in gears

Dr Nancy McGuire - Greases for slow and steady wind turbine bearings (2021)
Jane Marie Andrew - Fundamentals of wind turbines (2019)
Schaeffler - Wind turbine
Schaeffler - Spherical roller bearings (2018)
Micropitting
Stopping micropitting by using the right lubricant
Micropitting in wind turbines
Preventing micropitting and surface fatigue
Lubrizol - Meeting micropitting and materials compatibility challenges
Klüber - Synthetic gear oils (2018)
Klüber - Gear lubrication: Stopping micropitting
The effect of the surface roughness on micropitting
Proper lubrication is key to wind turbine longevity
Choosing the right wind turbine lubricant
Extending gear life with synthetic lubricants
Synthetic gear oil selection
Choosing between synthetic Lubricants and conventional oils
SAE - Traction coefficient measurement
Klüber - Lubricating gears with synthetic oils
Klüber - Specialty lubricants for optimum operation
Mobilgear SHC XMP 320 in wind turbines
Shell Omala S4 GX 680
Total Carter SH
Should you use synthetics? (links)

In addition to requiring oils to meet DIN 51517-3, Siemens MD requires an FVA 54 micro-pitting resistance test , dynamic foam testing and several stringent protocols for ensuring internal paint, elastomeric seal and liquid sealant compatibility.

6.1 Worm gears (PAG)

BAD ARTICLE (2018)

This is a surprisingly bad article.
The first, essential, question, completely ignored, is what gearbox it is. If it has worm gears (like in the picture), you MUST NOT use EP formulation. If you do, you might expect "increasing wear issues". If it is slow, it is likely to be a worm gearbox.
The picture is bad in itself, it is not a heavily loaded gearbox.
The second question is whether a good quality oil is used. A good ISO VG 680 oil at 52 °C will not be "dropping viscosity" unless you top up with wrong oil. A good mineral oil would be OK if it is not a worm gearbox.
In spur and helical gearboxes, synthetics are necessary only at temperatures above 90 °C. As mentioned, PAO is easier to use. However, it is WRONG to advise that flushing is not necessary.
You do not get pure PAO. It probably contains some ester to prevent additives dropping out. Ester will clean the machine that previously used mineral oil. That will clog the filter.
Seals are mentioned. PAO is happy with seals used with mineral oil. BUT if the machine is old, the seals are worn and might start leaking with PAO because PAO might not expand them as much as the mineral oil would.
For worm gearboxes, PAG is far superior to anything else. You don't need a heavier viscosity. In fact you usually use a lower viscosity PAG than you would with mineral oil.
If you don't use PAG, you should use the 150 year old formulation of steam cylinder oil with 5% lard in it.
I don't see a need for a cooling system.

Worm gear lubrication
The right way to lubricate worm gears
Klüber - Improving energy efficiency with proper gear oils
Klüber - Gear oils based on polyglycols
PAGs perform better in worm gears
Reducing wear particle generation (filtering and using PAG)
Roymech - Worm gear theory
The ins and outs of worm gears
Worm gears, also Misaligned - Scroll down
Avoiding worm gear problems
The effects of EP additives on worm gearboxes (2012)
Limitations of EP additives
The danger of EP additives on worm gearboxes (short video, 2018)

6.3 Open gears

Berly McCoy - Choosing the right open gear lubricant (2019)
Lubrication of open gears
Lawrence G. Ludwig - Applying open gear lubricants (2009)
Philip de Vaal - Open gear lubrication
Shell Malleus GL 3500

Lower wear is achieved with spray lubrication compared to dip lubrication. Graphite is known to promote abrasive wear.

Gear failures

(Beyond the scope of the book)

Gear failures
Mary Beckman - Gear failure analysis (2019)
Rexnord - Failure Analysis • Gears – Shafts – Bearings – Seals (1978)
Gear failure causes (short)
Analyzing gear failures (2012)
Analyzing gear failures (2001)
Recognizing gear failures
Bureau Veritas - Case study: Gear oil laboratory tests, water contamination (2017)

When receiving a new or reconditioned gearbox, open the drain plug and pump fresh oil through the system. This removes any contaminants that might not have been cleaned out during a rebuild or from a new machine. This will ensure your critical equipment has a better chance of reaching its life expectancy rather than coming to a grinding halt because of unforeseen contamination.

Surface finishing impacts how gears mesh in a mechanism by causing a build-up of tooth thickness. Not accounting for dimensional changes that may occur during surface finishing, case hardening or heat treatment can lead to poor performance and gear train failure.

Chain and wire rope lubrication

(Beyond the scope of the book)

Jeffrey E. Turner - Improving oven chain lubrication (2017)
John L. Wright - Chain lubrication in drives and conveyors (2002)
LE - Chain lubrication
Advice for chain lubrication
Bearings, Belts and Chain - Care and maintenance of rolling element bearings
Bearings, Belts and Chain - Articles
Lubrication of high-temperature chains
Improving oven chain lubrication
Rotalube chain lubricators
R. David Whitby - Lubrication of wire ropes (2020)
Lou Honary and John Sander - Lubricants for wire ropes (2015)
Jeffrey E. Turner and Christopher Barnes - Wire rope lubrication (2002)
Lubricating wire ropes (short video)
Advice for lubricating wire ropes
Best lubrication methods for wire rope applications
Marine wire rope lubricator
Viper wire rope lubricator (video)
Viper wire rope lubricators

Wire ropes used in industrial and mining applications wear from the inside out. The individual wires that make up the cable bundles slide and rub against one another as the cable turns around the sheave and drum. Cables are generally lubricated during the manufacturing process. However, the "initial fill" lubricant injected between the wire fibers during manufacturing is quickly squeezed out once the cable is placed under load.
The lubricant should be replenished promptly after first use to assure that the exterior and interior surfaces remain coated with an oil film. Pressurized lubrication collars can be most helpful in accomplishing complete coverage while minimizing waste.

7. Greases (also 7.3, 7.5 and 7.7)

Grease life is not only determined by the operating conditions and bearing type. The grease type and grease quality are also very important. A good grease has a stable consistency, good shear stability, favourable bleeding and flow properties, and good boundary lubrication, including lubricity properties. The base oil viscosity should also be favourable for the speed and temperature.

Marc Oosterlinck about greases (2021)
Dr Nancy McGuire - Greases for slow and steady wind turbine bearings (2021)
Mary Moon - NLGI unveils new grease specs (2020)
Rich Wurzbach - 7 steps to trouble-free grease lubrication (2018)
InterflonUSA - What is the difference between oil and grease? (2018)
Wikipedia - Grease
Grease basics
TLT - Grease manufacture (2017)
TESTOIL - Grease fundamentals and analysis (webinar)
Grease construction and function
Mobil - Grease: Its components and characteristics
Calculating grease quantity, frequency
Different types of grease
Aesthetics in lubricating greases (2018)
Chapter in a book: Greases
Understanding lubricants Part I
Discussing greases - Scroll up!
Shell - Presentation for the mining industry
SKF - Understanding grease technical data
Grease additives
Grease selection (2018)
Timken - Selecting greases
Consider consistency when selecting grease
Step-by-step grease selection (2005)
Application is key in grease selection
Selecting a high temperature grease
Choosing a high-temperature lubricant
Choosing a high-speed grease
Nicolas Samman - Grease cleanliness: How clean should grease be? (2003)
Biobased greases (2014)
Mary Beckman - Can you grease a squeaky railroad wheel and still stop a train? (2019)
Low-noise greases (2012)
Food-grade greases
STLE - Grease volumes and frequencies
Machinery lubrication - Articles about greases
TOTAL greases
TLT - Grease problems and solutions (2019)
UE - Bearing inspection and lubrication
Grease analysis (links)
Grease thief for taking samples
Timken - Grease tests and limits --- and Commercial greases
Testing grease consistency with rheometer (2015)
ASTM D3527: Are we using the right system to measure the life of a wheel bearing grease? (2018)
Noria - Grease colour (short video)
Des-Case - Proper lubrication for greased bearings (Centralized application systems)
Storing grease to avoid bleeding

The bleeding rate, which is the bleeding per unit of time, should ideally somehow match the starvation rate. In the beginning of bearing operation, the lubricant film will be relatively thick and no additional feed of base oil is required. A too high bleeding rate will exhaust the grease at an early stage, leading to short grease life. If the bleeding rate is too low, the contacts will starve rapidly, leading to early damage.

When using automatic grease lubricators that are set for several months, draw a line and record the date at the level of the lube during each weekly inspection. This allows you to instantly spot a plugged or faulty lubricator.

Large, abrasive particles in grease may be more damaging than the same particles in oil because once the grease is applied, no opportunity exists for the contaminant particles to be removed; whereas in oil, the particles may be quickly removed by filtering. The particles in a grease sample may be scrutinized by dissolving the grease with a suitable solvent and then preparing a ferrogram. A mixture of toluene and hexane is effective at dissolving many commonly available greases.

Applying a nice, thin layer of grease to sliding surfaces such as boom slides, crane outriggers or any sliding surface can be a problem. By using a regular paint roller of whatever size fits your application (2-inch, 4-inch, etc.), you have the ability to roll a nice, thin coat of grease on the area instead of all over yourself. Paint-roller pans work great and are available with snap-on covers to keep grease clean until you need to use it.
Al Allen, Sundt Construction

Grease guns and systems

(Beyond the scope of the book)

Before installing grease into a new grease gun, consider disassembling the gun and cleaning it thoroughly. I have found metal shavings numerous times in different brands of new grease guns. The metal shavings appear to be from the manufacturing process of the grease gun. (John Flynn, RJ Reynolds Tobacco Co.)

Rich Wurzbach - Strategies for overcoming gravity’s impact on grease (2018)
Grease guns
Anatomy of a grease gun
Grease gun best practices (2012)
What should we consider before purchasing a grease gun (short)
How to calibrate new grease guns (short 2018)
The benefits of ultrasonic grease guns
SDT Ultrasound Solutions - Ultrasonic grease guns
Ludeca - LUBexpert ultrasound grease guns
Brad Jeffries - Centralized grease lubrication systems (2005)
Heinz Bloch - Lubrication best practices (2019)

7.1 and 7.2 Grease thickeners, polymers and compatibility

Liwen Wei, Novitas - Quantum leap in the manufacturing of polyurea grease (2020)
CHEMTOOL - Grease thickener characteristics (2020)
Grease industry trending toward calcium (2 January 2019)
Why certain greases are more popular (2018)
Castrol - Grease thickeners
Choosing a multi-purpose grease: Lithium complex or calcium sulfonate? (2018)
Advantages of using polyurea grease (short, 2018)
Polyurea greases (2014)

We see demand catching up with supply by 2024. Seventy-five percent of today's greases use lithium-based thickeners, and 8 percent of lithium produced in the world today is used for grease. This is expected to change dramatically, as the share will likely fall to 2 percent in the future.
Silke Brand-Kirsch, 2019

Polyurea greases have excellent oxidation resistance because they don't contain metal soaps such as calcium, lithium, etc., which are pro-oxidants to varying degrees. Therefore, they are widely used in lubed-for-life bearings.

Aluminum complex grease accounts for only 3 percent of total global grease production.
But aluminum complex grease could bring performance benefits in selected performance areas, including a high dropping point, excellent water resistance, good shear stability, very good oxidation stability, excellent pumpability, chemical resistance, non-toxicity and heat reversibility.
Applications where both water resistance and heat reversibility are important could include the steel, paper and automotive industries, as well as construction machinery and trailers.
Bela Toth, MOL-Lub Ltd

Aluminum complex grease are better than lithium and comparable to lithium complex. These greases can also be used as food-grade lubricants, unlike lithium or lithium complex greases.
Vijay Deshmukh

Calcium sulphonate thickeners
Calcium sulphonate water resistant greases
Diurea chemical structure
Polymers in greases - Go to page 20
Dow Corning Molykote silicone-based high-temperature greases
Dow Corning - Molykote G-900X Series high-temperature (220 °C) greases (2017)
Molykote G-900X Series greases for high temperature applications (2017)
Lynne Peskoe-Yang - Factors influencing how grease performs at extreme temperatures (2020)
Axel Christiernsson - The ability of a greases to withstand, reject or absorb water
Axel Christiernsson - The effect of water ingress on environmentally adapted greases (2017)
Evan Zabawski - Grease (in)compatibility: Just say 'No!' (short, 2019)
Rich Wurzbach - Grease compatibility (2017)
Rich Wurzbach - The risks of grease mixing (quite short 2018)
Understanding grease compatibility
Grease compatibility
Elba - Grease compatibility
Elba - Grease compatibility
LE - Grease compatibility
Mobil - Grease compatibility
Grease compatibility and innovations (2016 forum)
Practical experience with grease incompatibility

When converting from one grease to another, double check to make sure that your soap bases and oils are compatible. The short and simple way to do this is to have your supplier or an independent test lab perform a worked penetration test on a mixture of the greases. Mixing greases can change performance. More often, mixing leads to loss of consistency, but for some mixtures, hardening may occur. Mixing of greases can also result in lowering of dropping points and changes in oil bleed rate. Individual grease lubricants most often perform better than the grease mixtures.

While grease may darken due to harsh operating or environmental conditions, grease manufacturers use colour simply to identify the type of grease and to make it more appealing to consumers.
Noria

7.4 Grease lubricated rolling element bearings

Rolling element bearings (links)
Clay Allen - Implementing best practices for motor greasing (2018)
Jim Fitch - How grease kills bearings (2003)
Right re-greasing frequency (short video)
Developing an effective motor bearing re-greasing strategy
Timken - Applying lubricants correctly
The basics of an electric motor re-grease program
Michael Weigand - Rolling bearing lubrication for critical running conditions (2006)
Diagram: Re-lubrication intervals
Electric motor bearing greasing basics
Mobil - Guide to electric motor bearing lubrication
Initial fill grease quantity
SKF - Replenishment
SKF - Quick tool for re-lubrication calculation
SKF - Lubricator calculation program
Other SKF calculators
LubeCoach calculators
Prolonged bearing life through effective grease lubrication
Re-greasing: How grease kills
Noria - Dangers of overgreasing (2011)
Heinz Bloch - Lubrication best practices (2019)
UE - Ultrasound assisted lubrication basics (2016)
SDT Ultrasound Solutions - LUBExpert
SDT Ultrasound Solutions - LUBExpert brochure
UE- Ultraprobe 401 Digital Grease Caddy Pro
Rexnord - Greasing (contrary guidance)
Determining lifespan for lubed for life bearings
Grease-lubricated electric motors with grease relief valves (2017)
Stop pumping oil into bearing grease (2012)
Ultrasound Solutions - LUBExpert re-lubrication tool (2017)
Ultrasonic energy measurement to improve effective lubrication practice (2012)
Timken - FAQ
tribonet - What contributes to thicker grease films?
Enviropeel housing spray bearing protection
Rolling element bearings (links)
Rolling element bearing failures (links)
George Frey - Electric motors: Keep it clean, keep it dry, keep it tight (2017)

Temporary shear thinning at a high shear rate happens in greases but the base oil viscosity may be permanently reduced. This happens under extreme conditions, such as in the case of high pressure, where the viscosity is very high. These conditions occur in the EHL contacts of rolling bearings. That's why viscosity modifiers (VI improvers) should not be used in bearing (and gear) oils.

Outer-ring rotation causes very severe conditions for the grease in the bearing. The grease on the shields or covers is subjected to centrifugal forces exceeding the yield stress, resulting in the grease flowing continuously into the bearing and causing churning, heat development and high temperatures. Moreover, grease on the bearing outer-ring shoulders or seals will show accelerated oil bleeding. In the case of outer-ring rotation, the base oil/grease is easily lost, and good sealing is therefore a prerequisite.

Roller bearings require a softer grease than ball bearings (on a horizontal shaft). Angular contact ball bearings pump grease through the bearing from the small inner ring diameter side ("low side") to the larger inner ring diameter side ("high side"). In order to prevent this, ideally a stiff grease is preferred on the "low side" and a softer grease on the "high side." Vertical shaft applications require a stiffer grease to prevent grease falling into the bearing.

At very low temperatures, the tendency of grease to bleed decreases and the hardness (consistency) of the grease increases. This may ultimately lead to an insufficient supply of lubricant to the contact surfaces of the rolling elements and raceways so the normal lubricating ability of the base oil in the grease can be diminished. It will then be the grease in its totality that will lubricate. This will result in a high torque, which may cause slippage of the rolling elements and therefore wear. This point is called the low temperature limit (LTL).

When hand-packing roller bearings, wear disposable food-grade gloves. This has a two-fold effect. First, it helps keep your hands free from grease, but it also helps keep the bearing free from contaminants. Particles and chemicals on hands can lead to premature bearing failure. (Jason Throop, Sara Lee Corp.)

Advantages of oil mist systems:
In bearing applications where high contamination levels are a concern, consider converting grease lubrication systems to oil mist lubrication. Oil mist systems are slightly pressurized, helping to exclude contaminants. Use a pure mist system for rolling-element bearings and purge mist for gearboxes and journal bearings.
Noria's Machinery Lubrication I training

7.6 Grease-filled gearboxes

How not to lubricate a gearbox
Discussion: Grease for gearbox?
Mobilux EP 023
Using grease for gear lubrication

Grease-lubricated equipment should not be kept idle for long periods. The base oil in the grease could separate out and get drained from the thickener, which does not have any lubrication properties. Stop and think about all of your equipment to evaluate the potential risks of grease separation.

7.8 Grease or oil?

Can you replace oil with grease? (short)
Understanding lubricants Part II
Oil lubrication vs. grease lubrication (video)
Grease vs. oil debate
Is it advisable to use grease instead of lubricating oils?

8. Bearings (also 8.2)

Add oil circulation for greater reliability
The inner life of bearings, Part I: How lubrication really works
The inner life of bearings, Part II - Lubricant selection and application frequencies
Tribological design guide part 1: Bearings
Tips for better process pump lubrication
Is your bearing getting fresh grease? (2012)
Wikipedia - Plain bearings
A case study: Plain bearing failures
Self-Lubricating bearings (2017)
Bearing materials

Paper machines, spindle oils, sugar mills, Morgan and Danieli

Wes Cash - Lubricating paper machines (2017)
Castrol spindle oils
Castrol Hyspin Spindle Oil E 5
Mobil Velocite spindle oils
Sugar mill bearings
Castrol - Biodegradable sugar mill lubricant
Shell Morlina S2 BA oils for Morgan and Danieli

Clean, dry oil is essential to maintain healthy equipment life and prevent shut-downs.

8.1 Rolling element bearings

David Schaljo, NKE Austria - Considerations for choosing the correct rolling element bearing characteristics (2019)
Rachel Fowler / Xiaolan Ai, Timken - Bearing fatigue life and the advantages of virtual bearing testing (2019)
Wes Cash - Understanding bearings prior to lubrication (2019)
Dr. Nancy McGuire - Designing better bearings (2019)
MIT - Rolling bearings
Rexnord - Checklist: specifying bearings for beverage application
FAG - Rolling bearing lubrication
Klüber - Lubrication of rolling bearings (44 pages, 2011)
Klüber - Guide to proper bearing lubrication procedures (12 pages, 2017)
How rolling element bearings work
Bearing clearances and fits
SKF - Articles - Select Mechanical Maintenance (need to register)
Bearings, Belts and Chain - Care and maintenance of rolling element bearings
Bearings, Belts and Chain - Articles
Steven Katz - Five ways to prevent bearing failures (2012)
Bearing news - Articles
Lubrication of pumps
Tips for better process pump lubrication
Manual or automatic lubrication? How to decide
UE - Subsurface fatigue and bearing life (2013)
Gearbox bearing service life
Bernd Seidenthal, Rick Trichka - Understanding the importance of bearing clearance (2018)
Tribological bearing testing
Can WD40 be used as a bearing lubricant?
Using oil mist to lubricate process pumps at high temperatures
Graphene-based nano-lubricants
Nano-technology improves bearing performance
NSK develops automobile transmission bearing with solid lubricant film
A 'solid' concept for bearing lubrication
Grease lubricated rolling element bearings (links)

When a properly packed bearing starts up, there will be an initial rise in the temperature while the grease disperses throughout the bearing and the housing before falling off to a steady operating temperature. If the temperature does not drop, then there is too much grease in the bearing or there is a problem with the bearing fit.

Rolling element bearing failures

(Beyond the scope of the book)

Chris Wilson - 12 reasons why bearings fail (check list, 2021)
Tom Murphy - Predictive lubrication: Which bearings will benefit from correct lubrication today? (2017)
ISO 15243: Bearing damage classification
SKF - How to determine the true cause of premature bearing failure (2019)
Bennett Fitch - 8 lubrication failure mechanisms for rolling-element bearings (2018)
Dr Wilfred T. Tysoe and Dr Nicholas D. Spencer - ZnDTP alone as a primary suspect in the formation of white etching cracks (2019)
Rexnord - Failure Analysis • Gears – Shafts – Bearings – Seals (1978)
How to determine bearing system life
Lubricant failure is bearing failure
UE - The 50 failure modes of electric motors (2014)
Determining the cause of bearing failures
Common causes of bearing failure 1
Common causes of bearing failure 2
Common causes of bearing failure 3
Hansford Sensors - Identifying bearing failure at an early stage (Accelerometer, 2018)
UE - How subsurface fatigue leads to bearing failure (2013)
Noria - Possible causes of a noisy bearing (short 2018)
William R. Finley and Robert R. Burke - Trouble shooting bearing currents (2000)
Electrical fluting: a current passes through the bearing
Shaft currents can have a destructive effect on electric motor bearings
Warning signs of a bearing failure
Bearing failures
How contaminants influence bearing life (2012)
Macpherson curve graph: Effect of oil cleanliness
ISO cleanlines versus time to failure
Deleterious particles in lubricating greases, Part I
Deleterious particles in lubricating greases, Part II
Deleterious particles in lubricating greases, Part III
Oil cleanliness (links)
Water contamination (links)

A bearing may fail for a number of physical reasons, such as wear due to (abrasive) contaminants either from external or internal sources, or from catastrophic collapse of the cage. In the bearing industry, however, attention has been focused largely on two principal causes. Historically, failure from fatigue of one of the raceways leading to spalling was the first mechanism considered. By contrast, the second mode of failure concentrated not on the materials of the raceways and rolling elements but rather on the lubricants, grease or oil, introduced to separate their relatively moving surfaces.
Grease Lubrication in Rolling Bearings

Surface-initiated fatigue in rolling bearings is much more common than subsurface-initiated fatigue. It’s generally caused by inadequate lubrication. If the lubricant supply or lubricant selection is wrong, or if the lubricant is contaminated, the contact surfaces will no longer be separated by an appropriate lubricant film. Areas that are rough or uneven can shear over each other and break off. The surface becomes plastically deformed and sometimes smoothened. Micro spalls occur and, in turn, grow to larger spalls. How to avoid it?

Lubrication condition is the key.

• Make sure that the appropriate grease is being used for the bearing.
• Be sure that a sufficient amount of lubricant is used.
• Follow the bearing manufacturer’s replenishment/overhaul intervals.
• Be sure that adequate sealing is used.
SKF

The top 10 causes of bearing failures:

1. Lack of lubrication training
2. Lack of lubrication-application engineering
3. Poor housekeeping (lack of order and cleanliness)
4. Over-lubrication of bearings
5. Under-lubrication of bearings
6. Use of dirty or contaminated new lubricants
7. Infrequent oil/filter changes
8. Bearing lubricant contaminated with an incompatible lubricant
9. Bearing lubricated with the incorrect lubricant
10. Bearing mounted out of square or misaligned when set up

Note that nine out of 10 items on this list are due directly or indirectly to ineffective lubrication practices.

Ken Bannister

8.4 Steam turbines (see varnish below)

Book: Turbine lubrication in the 21st century
Chapter in a book: Turbine lubricating oils and fluids
Chapter in a book: Turbine oils
Steam turbine oils: what you should know (2007)
Rob Profilet - A key factor in system reliability
Rob Profilet - Turbine oils, a key factor in system reliability (webinar)
LE - Steam turbine oil challenges
How to select and service turbine oils
Steam turbine lubricating oil characteristics
Fluitec - Turbine oil selection
Fluitec - Look beyond the specification sheet when selecting turbine oils
Performance evaluation of turbine oils
Mobil - Turbine oil condition monitoring
Jennifer Yeadon - Steam turbines and the battle for good demulsibility (2019)
ExxonMobil - How to select and service turbine oils (2006)
Fluitec - Triple your oil life through anti-oxidant replenishment
Optimizing turbine performance and longevity through a proactive maintenance approach
TESTOIL - Turbine oil analysis (some comments confusing = ignore them!)
Lubricant analysis in steam turbines
The surface tension test - is it worth resurrecting?
Electrostatic discharges in lubricants
Dangers of electrostatic discharge in engine oils
Electrical conductivity of oil
Identifying turbine oil cleanliness levels
Oil conditioner reduces bearing wear, downtime
Oil cleanliness (links)
Room for improvement (2011)

Varnish

Varnish is a thin, hard, lustrous, oil-insoluble deposit, composed primarily of organic residue.

IoT Diagnostics - IoT advantage in electrostatic varnish elimination (2019)
Varnish basics
Will varnish vanish? (2018)
Learn Oil Analysis - Varnish is like cholesterol in your machinery (2018)
Varnish mitigation: Effective fluid analysis and varnish-removal options (2018)
Lubricant varnishing and mitigation strategies (2014)
Oil Filtration Systems - Varnish contamination in hydraulic and lube oil systems
Fixing varnish (2008 discussion)
10 things you should know about varnish
Measuring and treating varnish formation in turbine oils
C.C.Jensen - Removing varnish from Group II turbine oil having ashless additives
University of California / Chevron - Varnish removal using chemical flushes (2018)
What is varnish? Function of antioxidants
Mechanisms of varnish formation and implications for the use of varnish-removal technology (2017)
Best strategies for managing varnish
Vanishing varnish
Y2K Filtration - Mitigating soluble varnish in critical systems (2018)
Catching varnish before it costs you (2006)
Reducing the varnish tendency of a Group II base oil by increasing the solvency
The new ASTM Standard for varnish potential
MPC Lubricant varnish potential test (video)
When to test varnish potential (short)
Fluitec - Membrane Patch Colorimetry (MPC) test ASTM D7843
EPT - MPC varnish potential testing ASTM D7843 (2016)
How to detect varnish in turbine oils
Effective varnish removal from turbine lubrication systems
Balanced charge agglomeration for turbine oil purification
C.C.Jensen - Filtering excessive varnish formations
ISOPur Fluid Technologies, Inc. - 55000 varnish-free hours using BCA oil purification
ISOPur Fluid Technologies, Inc. - 55000 varnish-free hours using BCA oil purification GE 7FA turbines
Soluble varnish removal (SVR) - Lube oil varnish removal success
Varnish and soluble varnish removal (SVR)
C.C.Jensen - Varnish removal
C.C.Jensen Varnish removal unit
Wear Check - Measuring and treating varnish formation in turbine oils
TESTOIL - Varnish potential analysis
TESTOIL - Varnish potential analysis report
Methods of varnish analysis (links)
Kleentek electrostatic oil cleaners
OILKLEEN electrostatic filtration system (YouTube videos)
Clean solution: Varnish removal by a new additive in fluid
Hydraulic oil additive package designed to combat varnish deposits

9.1 Air compressors, coalescer filters

John CumminsJenna Van Rensesslar - Air compressors and how they are lubricated (2020)
Wikipedia - Gas compressor
Russell Hattingh - Which compressor type to use – screw or reciprocating? (2019)
Different types of compressors
How reciprocating compressor works (video)
Wikipedia - Reciprocating compressor
Reciprocating compressors (2005)
Wikipedia - Rotary screw compressor
Mobil - Oil flooded rotary air compressor
Evaluate a rotary screw lubricant before you buy
Compressed air tutorial
Compressors (animated)
Compressor lubricants
Compressor oils by manufacturer
Mobil Rarus 400
Castrol compressor lubricants
TOTAL compressor lubricants
Mobil Rarus 800 diester
Mobil SHC Rarus Series
Mobil SHC Rarus 46
Wikipedia - Buna-N material for seals
Discussion: PAG vs. ester in compressors
Coalescing filter
Compressed air filters
Coalescing filter
Advanced analysis of reciprocating engines, compressors and gas pipelines
Compressed air for food plants (pdf)
Wikipedia - Diving air compressor
MACO (Gardner Denver) - Brochures: Breathing air solutions

While many compressors will run well at an ISO code of 17/14/11, if the compressor is highly critical, the target may need to be reduced to 16/12/10.

9.2 Vacuum pumps

Wikipedia - Vacuum pump
Vacuum pumps (dictionary entries)

9.3 Compressors for other gases

Choosing a safe lubricant when working with oxygen or reactive gases
Halocarbon - Source for fluorochemicals and inert lubricants

9.4 Refrigeration compressors

Refrigeration compressor lubrication
Oil in refrigeration systems
Refrigerant reference guide
Refrigeration oil
Compressor protection starts with a knowledge of refrigerant-oil basics
Naturals get new push at Atmosphere America
Wikipedia - Vapour-compression refrigeration
Wikipedia - List_of_refrigerants
Wikipedia - Chlorofluorocarbon
Refrigeration lubricants: Transitioning to new refrigerants
Oil management
Wikipedia - Polyol ester
Synthetic refrigeration oils - humidity related difficulties and solutions
Field and laboratory evaluations of lubricants for CO2 refrigeration
DuPont - Lubricant selection guide
Fuchs Refrigeration oils
Mobil - Refrigeration lubricant selection for industrial systems
Mobil-branded refrigeration lubricant selection guide for industrial systems
Mobil EAL Arctic series
Mobil EAL Arctic series (Product data sheet)
Mobil SHC™ Gargoyle 80 POE for carbon dioxide refrigeration compressors
Shell Refrigeration Oil
Shell Refrigeration Oil S4 FR-V
SUNISO GS Oils
TOTAL refrigeration oils
Vescolub refrigeration oils - See oil selection
Bitzer B5.2 lubricant for ammonia systems (2011)
Bitzer - Retrofitting R22 systems to alternative refrigerants (2011)

The Shell Clavus 68 was a naphthenic oil recommended for all types of refrigeration systems such as ammonia, and CFC and HCFC refrigerants e.g. R-11, R-22, R-500, R-502, R-22, and R-123. The Clavus oils were not recommended for use with HFC refrigerants such as R-134a.

Shell Refrigeration Oil S4 FR-F 68 is a synthetic polyol ester base fluid that is recommended for use with R-134a and other HFC refrigerants and blends. According to the literature, it is not recommended for use with other refrigerants such as R-22.

Shell Refrigeration Oil S4 FR-V 68 is a synthetic refrigeration lubricant based upon alkylated benzenes. It offers a universal solution to the lubrication requirements of most refrigeration compressors and is compatible with all commonly used refrigerants such as R-22 with the exception of HFCs such as R-134a. However, S4 FR-V 68 base stock is not compatible with Clavus 68 and if you are switching you need to thoroughly flush the system including lines and pump to prevent compatibility issues.

Hydraulic systems

(Beyond the scope of the book)

Brendan Casey - Maintenance of hydraulic equipment
Hydraulics vocabulary - Scroll down
Basics of hydraulics
Fundamentals of hydraulics (video)
Fluid power basics
Wikipedia - Hydraulic pump
Hydraulic pumps
Al Smiley - Troubleshooting hydraulic pumps (2018)
Al Smiley - 5 steps for more effective hydraulic troubleshooting (2018)
Vane pump failures
Restriction at the pump inlet - discard the suction filter
How hydraulic machines work
How Caterpillar backhoe loaders work
Hydrostatic transmissions
Understanding hydrostatic transmissions
Troubleshooting hydrostatic systems (2016)
Hydraulic accumulators
132 cardinal sins of hydraulics
Top 5 hydraulic mistakes and best solutions (2016)
Six costly mistakes most hydraulics users make
Tests to increase the reliability of hydraulic systems (2016)
Putting the brake on water hammer in hydraulics
Al Smiley - Best ways to eliminate hydraulic oil leakage (2017)
Kevan Slater - Detecting and managing hydraulic system leakage (2001)
3 ways to detect cavitation wear in hydraulic systems
Cavitation or aeration? How to tell the difference (2017)
Controlling aeration in hydraulic systems
Controlling hydraulic oil temperatures (2016)
Causes of darkening hydraulic fluid
Why hydraulic oil changes colour
Petro Canada - The fight against sludge
11 simple steps for flushing a hydraulic system
Pulsating hot oil flushing technology
Understanding filter debris analysis
Electrostatic discharges in lubricants
Al Smiley - 4 things every hydraulic troubleshooter should know (2018)
ACE - How to avoid hydraulic troubleshooting mistakes
Al Smiley - Troubleshooting hydraulic proportional valves (2017)
Three ways to reduce hydraulic shock
Failure mode and effects analysis (FMEA)

It is possible, but not desirable, that a big machine, like a Komatsu PC1250-7 hydraulic excavator, of this size, with its large number of conductors and connections could lose 5% or more of tank oil volume per annum through slow leaks; weeps and drips.

When it comes to sizing a hydraulic reservoir, my motto and advice is the bigger the better. Because the greater the tank volume the longer the dwell time the oil has to give up contaminants - particles, water and particularly air. Size DOES matter.
The rules of thumb for reservoir size - and that's all they are - differ for open and closed circuits. For open circuits the general rule is a tank oil capacity of 3 to 5 times the flow of the pump(s) per minute plus a 10 percent air cushion. For HFC and HFD fire-resistant fluids the general rule is 5 to 8 times pump flow per minute.
These ideals are easy enough to achieve on a stationary hydraulic machine in an industrial setting. In a mobile application it's a lot harder due to space and weight restrictions. For this reason, 1.5 to 2 times pump flow-rate is often a more realistic target for mobile machines.
Realistic, but not necessarily ideal. So, for example, if I was designing a mobile hydraulic machine and it was possible to squeeze in a tank volume of say 2.5 times pump flow rate per minute - I'd definitely do it. Like I say, the bigger the better.
That takes care of open circuit systems. But what about closed circuits (hydrostatic transmissions)? If the transmission pump has a flow rate of 100 gallons per minute, should the target tank volume be 300 to 500 gallons? No, that would be overkill. The flow rate of 100 gallons per minute is not passing through the tank. It is circulating in the transmission loop - pump to motor and back to pump.
But the charge pump on a hydrostatic transmission is open circuit, right? So how about 3 to 5 times the flow-rate of the charge pump per minute? If the transmission pump has a maximum flow-rate of 100 gallons per minute, then the charge pump would need to have a flow rate of at least 20 percent of that or 20 gallons per minute. Based on the 3 to 5 times rule, that equates to a tank volume of between 60 and 100 gallons. Certainly no harm in having a tank that size - if it can be accommodated.
Once again, in a mobile application, 1 to 2 times charge pump flow per minute is probably more realistic. And even that's extremely generous compared to what some hydrostatic transmission manufacturers recommend. Here's what Sauer-Danfoss recommends for their Sundstrand 90 Series transmissions:
"A suggested minimum total reservoir volume is 5/8 of the maximum charge pump flow per minute with a minimum fluid volume equal to 1/2 of the maximum charge pump flow per minute. This allows 30 seconds fluid dwell for removing entrained air at the maximum return flow. This is usually adequate to allow for a closed reservoir (no breather) in most applications."
Well, 30 seconds of dwell time isn't much. And unless I've been living in a cave all these years, closed or pressurized reservoirs are the exception rather than the norm. So while having a definitive recommendation like this from the manufacturer is reassuring, I'd say 1/2 to 5/8 of charge pump flow per minute is being ridiculously stingy in the majority of closed-circuit applications.
Brendan Casey Immersion elements intended for heating water usually have a heat density of 40 watts per square inch (6 watts per square centimetre). But this heat density is too high for heating oil. And as a result, the oil that comes into contact with the element burns or carbonizes.

To avoid burning the oil, the heat density of the element must be no higher than 4.5 watts per square inch (0.7 watts per square centimetre).

So if you have any hydraulic power units fitted with tank oil heaters, it might be wise to check the heat density of the unit installed. And if you ever need to install a tank heater, as well as keeping the heat density limitation in mind, here are the formulas to help you correctly size the unit:

kW = [Oil Volume (liters) x Temperature Change (deg-C)] / [35 x desired heating time (minutes)]

kW = [Oil Volume (gallons) x Temperature Change (deg-F)] / [13.3 x desired heating time (minutes)]

For reasons that should now be obvious, it's a good idea not to heat the oil too fast. For this reason, allow at least 60 minutes to get the oil up to the desired temperature.
* * *

Baffles are an important component in a hydraulic reservoir. They allow the fluid time to cool, de-aerate and settle out water and dirt. A good rule of thumb for residence time in a reservoir is three to five times the pump output. If the system is highly contaminated, residence time may be 10 times the pump's gallons/litres per minute. Baffles are used to prevent fluid just returned to the tank from passing directly back to the pump inlet. For a number of reasons, a longer transit path is considered beneficial; it encourages better heat conduction from the fluid, better contamination and air separation, and better mixing with the bulk fluid. This is usually accomplished by separating the inlet and outline by as long of a flow path as feasible.

Suction line leaks can cause air entrainment and problems such as excessive aeration, air lock, pump cavitation, poor lubrication and premature oil degradation. While a pinhole-sized suction line leak can be hard to find, using a small amount of shaving foam sprayed over the suspected leak area can indicate the source of the problem, as the foam is drawn into the line. This method should not be used for large leaks, and care should be taken not to use too much soap, since this can cause contamination of the lube, resulting in foaming and aeration problems and poor demulsibility.
Cavitation can have several root causes. Some relate to system and component design issues and others are more service related. Cavitation occurs when either air or vapor bubbles form in the suction line fluid and are subsequently emploded in the pump by the pressured oil. This leads to microjets of oil pounding and eroding adjacent surfaces. Below is a list of possible contributing causes of cavitation:

1. Tank design issues. Turbulence in the tank churns the air into the oil or simply doesn't allow air to be released from the oil. This can be caused by plunging oil returns, low oil level, a tank that is too small, lack of proper baffling, etc.

2. Suction-line leaks. Leaks between the tank and the pump can introduce air. Often this is associated with the shaft seal at the pump that allows air to leak in.

3. Suction-line restriction. Sometimes suction lines are too long, too narrow or they are simply plugged (for example, a plugged suction strainer).

4. Insufficient head. Depending on oil viscosity and suction line conditions, the pump must be located at a sufficiently low elevation to enable oil to flow readily from the tank to the inlet port of the pump.

5. Air release problems. As oils age and become contaminated, air release properties become impaired. This simply means that once air bubbles form, they stay locked into the matrix of the oil and don't detrain out of the oil in the reservoir. Moisture contamination and oxidation are known precursors to this problem, among many others. ASTM D3427 is a test for air release properties.

6. Water vapor. When hot oils become contaminated with water, superheated seam will form vapor bubbles in the oil.

7. High viscosity. When reservoir temperatures are too cold, during wintertime startup conditions for example, the viscosity may be too high to enable proper oil flow in the suction line and into the pump. Other causes of high oil viscosity can lead to the same problem.
Jim Fitch, Noria

If oil is not used to do work but to transfer heat, properly formulated hydraulic fluid is not necessary and is not used. The oil could be just low viscosity base oil. There is a word describing the arrangement:
hydronic (hī-drŏnˈĭk) - relating to a heating or cooling system that transfers heat by circulating a fluid through a closed system of pipes.
If the system is correctly designed, that means hot oil is not exposed to air, base oil is sufficient under normal conditions.

10. Hydraulic fluids

Tim Smith, Lubrizol - Sustainable practices through efficient hydraulic flow (2020)
Schaeffer- Maximum efficiency hydraulic fluids (2018)
Eaton - Selecting fluids for hydraulic pumps (2016)
Wikipedia - Hydraulic fluid
Evonik - Hydraulic fluids (2017)
Hydraulic fluid selection and maintenance (2015)
Selecting hydraulic fluid
Machine Design - Hydraulic fluids
MachineDesign - Fluid performance factors
Performance classes for hydraulic oils
Hydraulic fluids
Hydraulic systems and fluid selection (2002)
LE - Hydraulic fluid selection and maintenance
Brendan Casey - Importance of viscosity (2005)
Does your hydraulic fluid provide enough protection?
Why hydraulic oil is different
Which hydraulic oil should I use?
Advantages of zinc-free hydraulic oils (US perspective)
Important considerations for choosing hydraulic fluids
Brendan Casey - Choosing the right hydraulic fluid
Brendan Casey: Limits for hydraulic fluids
Understanding hydrolysis and hydrolytic stability
Testing hydraulic fluids
A hydraulic fluid choice - showing the optimum operating range...and references
Peter Mainka's hydraulic views
A hydraulic fluid saves energy
How to improve hydraulic efficiency
Hydraulic oil can make a major difference to power consumption
Bosch Rexroth - Validated hydraulic fluids increase the service life of the hydraulic system (2018)
Bosch Rexroth - Fluid rating list (2018)
Bosch Rexroth - Reliably increase the service life of hydraulics (2015)
Bosch Rexroth - Press release (2016 - click to download fluid rating list)
Bosch Rexroth - Data sheet No. 90235: Rating of hydraulic fluids (2015)
Chevron hydraulic fluids
Shell Tellus brochure
Shell Tellus S (original version)
Rhein Chemie - dispersant and emulsifying type (HLPD) additive pack
Afton - HiTEC 521 Anti-wear hydraulic additive package
10.2 Oil cleanliness (links)
Particle counting, cleaning oil, filtration (links)
Oil filters (links)
Flushing (links)

The only lasting solution is to get the machine's operating temperature down to below 85 °C.
Allowing a hydraulic machine to run too hot is the most costly mistake a hydraulic equipment owner can make.
Brendan Casey

Use the right hydraulic fluid, keep it clean and dry, and replace it when it does not look good. You can often see and smell the general condition of a lubricating oil.
Petr Vavruch

10.1 Fire-resistant fluids

Bennett Fitch - When to use fire-resistant hydraulic fluids (2018)
A page in a book: Fire resistant fluids in turbines
Chapter in a book: Fire resistant fluids in turbines
Fire-resistant fluids (pdf)
Fire-resistant fluids (text)
Rexroth - Axial piston units for use with HF Fluids
Mobil - Fire-resistant fluids, conversion and compatibility
Using water-in-oil emulsions
Advice for using water-in-oil emulsions
Measuring emulsifier performance
Water-glycol fire-resistant hydraulic fluids
Dow's UCON - Water-glycol hydraulic fluids
Fire-resistant HFC hydraulic fluids
Quaker QUINTOLUBRIC fire-resistant fluids
Quaker QUINTOLUBRIC fire-resistant hydraulic fluids (video)
Phosphate esters
Electrohydraulic fluid
Phosphate ester, the true fire-resistant fluid (video)
Seal compatibility - Select Pyrogard
Maintenance of fire-resistant fluid (phosphate ester) 2007
Maintenance of fire-resistant fluid (phosphate ester) 2013
Large system fluid change (2017)
Controlling the acid in phosphate ester-based hydraulic fluid
Heat of combustion, flash point, autoignition temperature of PAG
Effects of water on PAG
FM Global

Factory Mutual, FM Global, is a US-based mutual insurance company which assists businesses worldwide. The company carries out its own scientific research, approves fire protection equipment (FM Approvals) and publishes its own installation regulations (FM Data Sheets - FMDS). FM Global assesses the risks of its policy holders, appoints a project engineer to produce protection system recommendations and, upon completion of the work, the project engineer is brought in to verify that the protection provided complies with his recommendations. FM Data Sheets are recognised standards for fire protection in industry. They are available to consult free of charge and other insurers may use them as their standard.

Given a high enough temperature, all hydraulic fluids can be ignited when coming into contact with an ignition source. The real test of fire resistance is whether a fluid is capable of self-extinguishing. The ability to self-extinguish can make the difference between a momentary flash that causes no harm and a conflagration, which results in injury to personnel and/or loss of equipment. Only phosphate esters offer such fire-resistant characteristics.

Trixylenyl phosphate fluids are used in large steam turbines of nuclear power plants where temperatures reach high enough to ignite mineral oils. These synthetic fluids are extremely difficult to ignite and inherently self-extinguishing. Besides their high oxidative and thermal stability, they can contain water and have good hydrolytic stability.

Viton is compatible with all fire-resistant fluids, except HFC fluids.

11. and 13. Lubricant storage and storage life (shelf life)

Avoid the use of galvanized steel storage and dispensing containers. The zinc in the galvanizing can act as a catalyst to promote lubricant oxidation and premature depletion of critical additives. There are many other types of more chemically stable platings for metal containers. Stainless steel or plastics are also suitable alternatives.

Lubricant storage life
Mobil - Shelf life
Chevron Marine - Shelf life

12. Transformer oils

South Africa: New transformer monitoring technology gives speedy results (2020)
Rapeseed natural ester fluid for Extra High Voltage transformer (2020)
Cargill natural ester fluid for South African electrical grid (2020)
Wikipedia - Transformer oil
The transformer and its oil
Transformer selection and maintenance
Hendrik Cosemans - Properties behind effective transformer oil cooling (2013)
Specifications of a transformer oil
Intertek - Transformer oil tests
SGS - Transformer oil analysis (2016)
Testing transformer oils (2013)
Dissipation factor
Capacitance and dissipation factor (2016)
What is furan analysis in transformer oil? (2018)
Interfacial tension (2016)
Interfacial tension
Accurately monitoring interfacial tension of transformer oil quality (2018)
SDMYERS - Choosing gas monitors to fit the specific needs of your equipment (2019)
GlobeCore - Oil regeneration extends transformer life by 20 years
Nynas transformer oils
Shell Diala GTF transformer oil
Vegetable oil as insulating fluid for transformers
Natural ester oil application in liquid filled transformers (2.5 Mb)
Maintenance free monitoring with the Vaisala Optimus OPT100 DGA (2018)
EPA - PCB information leaflet (2018)
PCB: Fire-resistant transformers food processing for installations (1967)

The oil in a transformer serves as an insulating medium which is used for cooling, protecting the paper and for analysis. Regular oil analysis is considered one of the most critical activities that will assist in monitoring the condition of the transformer and facilitate predictive servicing. The oil analysis regime should include dielectric strength, water content (Karl Fischer), acidity, interfacial tension and dissolved gas analysis (DGA) that provides a clear indication of internal failure conditions. The oil should be analysed to determine if polychlorinated biphenyls (PCBs) are present. Furanic analysis should also be done as this will determine the cellulous breakdown products in the oil and give an indication of the life expectancy of the insulation in the transformer. High moisture will result in dielectric breakdown.

14. Machine tools

Lathe lubrication
Way lubricants
Elco slideway lubricant additive
Scroll down to BASIC LUBRICATION articles
Test kit for metal working and steel plant fluids

15. Cutting fluids, metal cutting, grinding

Metal working fluids
Tutorial on cutting fluids
Cutting fluids
Wikipedia - Cutting fluid
Noria - Choosing metalworking fluids (short)
Properties a cutting fluid should have
Cutting fluids (coolants)
TLT - Formulating water-based metalworking fluids (2017)
How metal working fluids can boost machine shop productivity
Optimising metalworking fluids - good practice guide
Minding the metalworking fluids
Jane Marie Andrew - Condition monitoring of metalworking fluids (2019)
Metalworking fluid troubleshooting guide
Guidelines for selecting additives in metalworking fluids
Amines 101 for metalworking fluids
Chlorinated paraffins
ILMA clarifies confusion over anticipated EPA action on chlorinated paraffins
Metal working fluid microbiology (2018)
Dr. Neil Canter, TLT - Metalworking fluids: The quest for bioresistance (2019)
Metalworking fluid discovery of the century?
Castrol cutting fluids
Fuchs soluble cutting fluids
Minimum quantity lubrication
Minimum quantity lubrication reduces total costs of operation (2017)
Selection and use of grinding wheels (1965)

Lead enhances metal machinability. Traces of lead are added to steel, aluminium and copper alloys for rapid, accurate and efficient machining with currently available tools and metalworking fluids. The lead reduces friction between machine tools and parts, allowing faster production of parts and lower energy consumption.

Chlorinated paraffins are chlorinated alkanes that have carbon chain lengths ranging from 10 to 38, with varying degrees of chlorination. Those with lengths from C14 to C17 are classed as medium chain; from C18 to C20 as long chain; and C21 and higher as very long-chain. CPs are used in metalworking fluids as extreme-pressure agents, especially for difficult drawing, forming and removal operations. Metalworking fluids thus fortified are often used to machine titanium alloys, stainless steels and other metals, because they protect tools and components from friction, wear and overheating at high speeds and intense pressures.
Chlorinated Paraffin Industry Association Executive Director Andrew Jacques noted that "because medium-chain CPs similar to the [pre-manufacture notice] substances have been manufactured, processed and used for the uses described in the [pre-manufacture notices] for more than 40 years, manufacture, processing, distribution in commerce, use and disposal of the [pre-manufacture notice] substances in accordance with the provisions of the TSCA section 5(e) order do not create an unreasonable risk of injury to health or the environment."
George Gill

16. Rust preventives

CHEMTOOL - Vapour phase corrosion inhibitor (2020)
Protect equipment in short-term storage, stand-by or decommissioned
Preserve equipment by oil mist lubrication
Wikipedia - Rust
Keep rust and corrosion from crippling your productivity
Rust protection oils

Oil mist is effective in protecting stored machines. The Caltex Thailand Refinery added a new dimension to the capabilities of oil mist lubrication by using it to preserve rotating machines while they were sitting in storage yards. The machine manufacturers connected tubing from the oil mist connections on the machines to connectors on the sides of the shipping crates. A temporary system was connected to the crates upon their arrival to the yard. Typically, upon startup, there are numerous bearing failures. In this case, there were virtually none.
Douglas Branham, Lubrication Systems Co.

Try using a vacuum-packaging unit (the kind used for storing food for freezing) to help with parts storage and preservation. This quick and simple method can be used to keep items clean and dry. Parts can be sealed in plastic with a desiccant bag for good measure. It can also be used to keep small parts organized until they are needed, such as a matched set of coupling bolts, springs or electronic parts.
Van Richard, Georgia Gulf

REVISION 3

Answers to REVISION 3 (link)

18. CHALLENGE

Hint No. 2 (link)
Hint No. 3 (link)
CHALLENGE solution (pdf)

ANSWERS

Answers (link)

The following sections, except 'Oil cleanliness', are not covered in the book

Fuels

Managing waxy marine fuels (2020)
Donaldson - The effect of hard particle wear on diesel injectors (2015)

Suppliers' information, approved and recommended lubricants (no endorsements, for information only)

Lubricating equipment catalogue
PLANT ENGINEERING - Products by oil companies (June 2019)
Product equivalents
LubriTec - Synthetic SAE 50 lubricant cross reference
B’laster Corporation - PB Penetrating Grease
CASE - Commercial / Farm / Earth-moving lubricant recommendations
Castrol
Castrol
Castrol oil chooser
Castrol unveils VW's first 0W-20 engine oil (see also VW below)
Caterpillar lubricants (July 2014)
Caterpillar commercial diesel engine fluids (September 2014)
Cepsa lubricants
Chevron promotional (2019)
Chevron industrial and fleet lubricants
Cummins approved product lists
Cummins issues new CES 20086 oils list
Cummins OilGuard extends oil drain interval for X15 Series heavy-duty engines
Cummins recommends fuel additives
Dow Corning - Molykote G-900X Series high-temperature (220 °C) greases (2017)
ELF announces 0w-20 oil for Volkswagen (VW 508.00 / 509.00) and Porsche (C20) (2017)
Engen lubricants
Eni product brochure download (interesting)
Evonik additives (VII, PPD)
FL Smidth - Key to lubricants
Fuchs’ Titan Cargo MAXX SAE 5W-30 meets Scania’s LDF-4 requirements
Functional products additives
dexos engine oils (9' video)
General Motors - approved dexos1 and dexos2 engine oils
dexos1 Gen 2 taking off (October 2017)
GM dexos1 Gen 2 licensed oils list now contains 168 oils (July 2017)
General Motors dexos1 April 2017 update
General Motors dexos2 licenses (2017)
General Motors - The new GM dexos2: It’s complicated (2016)
Generation Systems Inc - LUBE-IT software (2018)
Gill - Oil condition sensors (2018)
Gill - Oil condition sensors (2018)
Harvard - Filters, carts (2018)
IFH Group - Carts (2018)
Klüber
Klüber - Using water as a functional component in specialty lubricants (2018)
Klüber articles, e.g. Bearing lubricating procedures
Lubrizol additives
Mack Trucks - Approved oils
Mack Trucks announces extended oil drain interval for genuine oil
Mobil greases
Mobil product selector
Mobil - Optimum performance with energy efficiency built in
MOLYKOTE - Machinery problems solved by selecting products
NATO's lubricant specifications
Porsche launches motor oil for classic cars with air-cooled engines
Shell products
M Hussam Adeni - Shell products (2018)
Shell lubricants
Shell Rotella product selector
Shell recommendations
Shell unveils CK-4, FA-4 strategy
Spectro Scientific - Instruments (2018)
Swift Filters Inc (2018)
Todd Technologies Inc (TTI)) - Breathers (2018)
TOTAL lubricants
TOTAL industrial lubricants
TOTAL industrial greases (USA)
TOTAL industrial greases (UK)
TOTAL LHM PLUS hydraulic fluid for CITROEN
Valvoline - Synthetic petrol engine oil to combat carbon build-up (2018)
VW oils explained
Wolf releases OFFICIALTECH 0W20 LL FE motor oil for new VW engines

Lubricant monitoring, sampling and analysis

Monitoring equipment without special instruments and without laboratory samples

Oil analysis is not simply about a periodic sample pulled from a machine and sent to a laboratory. A lot of organisations today are empowering their maintenance staff and operators to do a certain amount of quick, on-site inspections and field tests. The concept of a frequent inspection, what is called a daily one-minute inspection, can far exceed the benefits of monthly or bimonthly oil sampling where very sophisticated laboratory testing is done.

Many equipment inspections are visual, and checking oil levels is the most common visual monitoring activity. Numerous potential machine failures are prevented by an attentive individual who notices a low oil level. Other valuable functions can also be performed as part of the visual inspection. Lubricant issues such as oil contaminated with water or other materials, badly degraded or oxidized oil, and excessive foaming, as well as other machine conditions including excessive vibration, loose belts, loose drive chains and loose or missing fasteners are all examples of what should be routinely documented and scheduled procedures.

In machinery condition monitoring, a decision on the condition of a machine is dependent on the nature of its signals. For example, if the machine produces excessive noise and vibration, one gets a clue that something is not normal with the machine. These signals are usually time varying and need to be understood because they carry the information from the machine to the decision system, which can be a developed software or a person.

Temperature is a very important parameter to be monitored, in particular for bearings and shaft couplings. Many instruments are widely used for temperature measurements. At high temperatures, when mounting or access to machines is a problem, non-contact instruments like pyrometers and thermal imaging cameras are appropriate.

While pulling a sample from a reservoir, an exceptional amount of air was found in the hydraulic fluid. The suction-side components were sprayed with mineral oil to locate where air was being ingested. The pump became quieter after the input shaft seal was sprayed. The sprayed oil was seen being drawn into the pump. A check of the pump revealed a worn bearing and shaft seal, which were attributed to oil contamination. The pump was replaced, and the source of contamination entry was located. The bottom line is to listen when your oil talks to you.
Mike Deal, Alcan Aluminum
Spell out just what the operator should do for proper equipment care, such as routine checks and records, or checking oil level and condition, removing excess dirt from the equipment, turning in equipment for oil changes and maintenance, and reporting any loose, damaged or deteriorating parts.
Keep operators conscious of the need for continuing inspection including: reporting worn or damaged tubing and hose, foaming or turbulence in the oil reservoir, signs of overheating, oil leaks, loose joints, worn seals, and any unusual noises that might mean cavitation, trapped air, or worn bearings and seals. Encourage the operator to note and report any slowdown of machine operating time that might be an early warning of future problems.
Fluid Power Maintenance and Troubleshooting

Des-Case - Visual lubrication inspection (2018)
Inspection 2.0 for early fault detection (2016)
Jim Fitch - The 5 states of machine inspection 2.0 (2017)
Noria - Condition monitoring with Inspection 2.0 (webinar)
The daily one-minute inspection (2007)
Shaun de Villiers - The daily one-minute inspection (presentation)
Utilizing your senses as Condition Monitoring tools
Checking the colour of the oil (short video)
Water-in-oil
Water contamination (links)
What's that smell? Using odour as an oil analysis tool
How to give your machine a physical (2005)
Regular inspection of critical lubrication parameters
How to troubleshoot anything
FUTURE: Move to IoT-based machine condition monitoring (2018)
FluidRX One Drop fluid analysis kit (patch)
Esco - Magnetic oil monitors
Deutz: Oil performance check (patch)
Jonathan Trout - Infrared thermography (2019)

Chemists might refer to the blotter spot test as paper chromatography. It dates back to the early days of the lubrication industry in the mid-1800s and is still used today. It has been utilized for a variety of different reasons, including to assess the condition and quality of oil.

In time-critical situations where real-time infrared thermography is impractical and thermocouple/recording equipment cannot be installed, consider temperature-sensitive tapes. These tapes are manufactured in a variety of sensing ranges and will clearly record the peak temperature that a machine area reached since the tape was first applied. A quick visual check is all it takes to read the "paper thermometer.
Mark Smith, Analysts Inc.

Oil and grease sampling

SUMMARY: Effective oil sampling

The sampling technique that gives the most representative sample is one in which the sample is taken from a pipe carrying oil scavenged from the wearing parts and before filtering. Clearly, it is necessary for the machine to be operational to do this. Care must be taken that the sample is representative of the complete system, i.e., that the scavenged oil has passed through all the wearing parts.

To achieve the most representative and 'trendable' information from oil sampling, follow these basic tips:

1. Samples should be collected when machines are running at normal operating temperatures, loads, pressures and speeds. This will ensure that insoluble and semi-soluble (dirt, water, and other debris) material is suspended evenly throughout the system.

2. Sample upstream of filters and downstream of machine components such as bearings and gears to obtain the best data. Sampling downstream from the filters should be performed if you wish to determine the effectiveness of your filtration system.

3. Document oil sampling procedures for each system - tools needed, line flushing requirements, sampling locations, sampling methods, and safety requirements are among some of the items to include in the written procedures. This ensures that each sample is taken in the same manner and from the same point. Procedures that are documented also help new employees quickly learn the process.

4. Properly flush sampling valves, devices, and hardware thoroughly prior to taking oil samples. To avoid cross-contamination, use a new sampling tube for each sample taken.

5. Make sure that oil samples are taken at the proper frequency and that the frequency is sufficient to identify problems. Sampling frequencies should be set specifically for a particular machine. Every machine is unique in its intended performance, condition, locality, operating environment, and maintenance schedule.

6. Forward samples immediately to the lab after sampling. Ideally, oil should be analysed within 48 hours of being sampled.
Trico Corporation

Bernie Hall - Step up your oil sampling program (2021)
Bennett Fitch - Representative oil sample: Part 1 - Sample bottles (2014)
Bennett Fitch - Representative oil sample: Part 2 - Sample extraction tools (2014)
5 considerations when selecting machines for oil analysis (2018)
TESTOIL - How to consistently collect a representative sample (webinar)
Oil sampling do's and don'ts
Advice for quality oil sampling (short video)
Sampling procedures
Proper bottle sampling technique (short video)
John Fitch - Clean oil sampling - how to sample oil without opening the bottle (1998)
Sampling instructions
Good oil analysis starts with good sampling practices
Noria - Sampling location - wet sump (video)
Sampling points
Sampling points (short video)
Live zone oil sampling (short video, 2018)
World-Class Oil Sampling - It is Possible
Noria webinar: Best practices for oil sampling
Oil sample extraction tools
Luneta - The hub of lubricant monitoring (2018)
Sampling is key to oil analysis accuracy
Tips for flushing your sampling equipment (short video)
Lubricant sampling design and implementation
Particle settling and oil sample agitation (2015)
Test yourself question
Hydrodynamics and oil sampling
TESTOIL - The importance of oil sampling on a-regular basis (2018)
Tools for effective grease sampling
Grease sampling methods outlined in ASTM D7718
Quick and easy test for grease conditions
How to obtain grease sample from pillow block bearing
Why you should inspect bearing grease discharge
MRG Laboratories - Grease sampling videos

When possible, don't take oil samples from cold systems. Samples that are consistently collected from cold systems will have altered concentrations of wear metals, contaminants and other insoluble suspensions. When at rest, anything heavier than the oil will begin to settle. It takes only two minutes for a 20-micron particle of Babbitt bearing metal to settle 1/2 inch in an ISO 22 bearing oil. If unavoidable, cold systems should be labelled as such.

With the proliferation of digital cameras, why not take a photograph of the oil sample (requires the use of a transparent sample bottle) and store the image in a trending software for comparative purposes. Record a new oil sample and use this as a baseline. Set the bottle against a white background such as a sheet of paper to maintain a consistent color comparison. You can also use the camera in other ways such as to record images of the machine and sampling point as a means of identifying it in the software or to record abnormalities.

Sampling frequencies

TESTOIL - Oil sampling frequency (4' video, 2020)
Bennett Fitch - Representative oil sample: Part 3 - Sampling frequency and location (2014)
Establishing oil analysis frequency (short, 2018)
Establishing effective sampling frequencies (Revised in the next link)
Establishing oil analysis frequency
The importance of machine criticality
Criticality analysis for machinery lubrication (2013)

The appropriate sampling frequency is determined by the nature of the machine, its use and how important early warning is to the user. Experience has shown that in many failures abnormal wear particles were present in the lubricant, indicating that the machine was defective from the start. The reasons for this are easy to see. Many failures are the result of improper assembly, a defective part or poor design. Such difficulties result in abnormal wear debris from the beginning.

Designing oil analysis programme, condition monitoring, standard test methods

Survey of practical experience with condition monitoring (2021)
Wearcheck bulletin
TESTOIL - Justify an oil analysis programme with ROI (short, 2021)
TESTOIL - Kickstart your oil analysis programme (39 pages, 2020)
Learn oil analysis - Resources
Jim Fitch - How to make your oil analysis program produce more alerts (2018)
Tips for understanding your oil analysis reports (very short, 2018)
Jeanna Van Rensselar - Thorough oil analysis (2019)
Bill Quesnel - Best practices for using oil analysis in lubrication management (2017)
Learn Oil Analysis - Why oil analysis matters (2018)
Managing effective fluid analysis: 10 steps to realize your return on investment (2018)
Noria - How to justify an oil analysis programme (short)
Noria - How to justify a lubrication programme (2018)
4 ways to improve your oil analysis program
How to avoid machine failures with routine oil analysis
Implementing world-class oil analysis (short video)
Chevron - LubeWatch oil analysis program
Why oil analysis programs fail (short video, 2018)
10 steps to create a world-class oil analysis programme
Strategies for lubricating heavy machinery (2017)
5 keys to a successful oil analysis program
Choosing equipment for oil analysis (short 2018)
Best practices for using oil analysis in lubrication management (2017)
Noria - How to get maximum value from your oil analysis program (webinar, available until 27 June 2018)
The benefits of route-based oil analysis
Selecting the right oil analysis lab (2016)
Oil analysis and its role in equipment reliability (2017)
FTIR oil analysis (2015)
Understanding the 'Rights' of oil analysis
Tracking the life cycle of your lubricants
Jim Fitch - How to measure the effectiveness of condition monitoring (2017)
A practical approach for evaluating oil analysis results with limit values
How to select machines for oil analysis (2015)
How to select the right oil analysis tests
Bennett Fitch - Engine oil analysis (2016)
Bureau Veritas - Case study: Gear oil laboratory tests, water contamination (2017)
Effective use of the patch test for simple on-site oil analysis
Is oil analysis a waste of time?
Predicting machine failure with oil analysis (short video)
The 'rights' of oil analysis
Six steps for more effective oil analysis
5 steps to best in class oil analysis
Oil analysis optimization
How to develop an effective oil analysis strategy
Setting up oil analysis programme
Do oil and coolant analysis together
Yellotec - Why you should think about having an on-site lab (2019)
Yellotec - Is it worth the investment of an oil analysis lab? (2019)

Because the viscosity of an oil is probably its single most important property, it makes sense to measure viscosity frequently, using on-site test equipment. However, like with all onsite equipment, it's important to understand how these instruments work and their relative strengths and weaknesses. When it comes to viscosity, there are two determinable parameters, absolute and kinematic viscosity. Kinematic viscosity measures the resistance of an oil to flow and shear under gravity, such as oil flowing through a funnel. Absolute viscosity, on the other hand, determines an oil's internal resistance to flow and shear. To visualize absolute viscosity, imagine the force needed to stir an oil using a metal rod.

The viscosity reported by your lube supplier and oil analysis lab is likely the kinematic viscosity, as determined by ASTM D445. There are two main reasons why your on-site measurements may not correlate directly with the lab data.

First, most on-site test equipment actually measures absolute viscosity, but calculates the kinematic viscosity by dividing absolute viscosity by density. Because the onsite viscometers don't actually measure density but rather estimate it from the oil's spec sheets, an error can occur when translating absolute viscosity into kinematic viscosity. The measure of the absolute viscosity is correct, but because the density of the oil is only estimated, the conversion to kinematic viscosity can become overstated. Contamination and oxidation, among other things, can cause an increase in the density of used oil.

Second, if your on-site instrument does not heat the oil to 40 degrees C, and most do not, you are likely determining the oil's viscosity at the temperature of the on-site lab (typically in the 20 degrees C to 25 degrees C range), and extrapolating, again using a software algorithm to determine the viscosity at 40 degrees C. This extrapolation can also introduce errors into the reported measurement due to changes in viscosity index of the used oil.

Despite these limitations (which are actually not negatives), when used properly, on-site viscometers make valuable additions to any on-site test program. As a general rule, always baseline your new oils using your own on-site viscometer to determine nonconforming used oil viscosities quickly and simply.
Mark Barnes, Noria

A major mobile equipment manufacturer estimated that an average of 53 percent of all engine failures are a direct result of problems with the cooling system. Periodic coolant analysis, including glycol content, pH, conductivity, inhibitor analysis, visual inspection and resistance to corrosion, may be as valuable as routine oil analysis in preventing failure due to the cooling system.

While oil analysis can't fix a failed machine, it can provide pre-failure alerts, both cautionary and critical. If a root cause is detected, such as the wrong oil, dirty oil or wet oil, these conditions can then be remedied quickly.

Robert Chapman - Oil condition monitoring keeps equipment healthy (2017)
Patrick Parvin - Choosing and implementing a successful condition monitoring programme (45' video, 2016)
Unified condition monitoring approach
PALL- Crixus fluid condition monitoring platform - moving from reactive to predictive fluid maintenance (2017)
UE- Remote monitoring platform to revamp PdM process (2017)
National Instruments - InsightCM for remote diagnostics (2018)
Improving maintenance strategy with online condition monitoring
Common mistakes in CM programmes

According to the Electric Power Research Institute (EPRI), online monitoring is the implementation of applications for monitoring, maintaining, and optimizing assets from a centralized location. Such monitoring becomes necessary in today's fast-evolving global economy for companies that rely on assets as they face increasing reliability concerns. Unexpected downtime and maintenance can lead to significant cost and safety repercussions that can easily affect a company's bottom line.

LE - Industrial application condition monitoring by oil analysis
LE - We have not replaced our gear oil in 8 years
Polaris - Make oil analysis an integral part of maintenance programme
Analysts, Inc. - Proper testing for maximum value and equipment condition information
Selecting machines for oil analysis
Selecting machines for oil analysis (discussion)
Improve gearbox reliability with oil analysis and contamination control
Laboratory analysis of a used-oil sample
Grant Dawson - Choosing the right diesel engine test package
Spectro - Oil analysis handbook 2014-08 (pdf)
Spectro - Clarify the mystery of in service oil analysis techniques
Test explanations
Oil analysis tests and their significance
Oil analysis test method standards
TESTOIL - Oil analysis lab test methods
Lubetrend - Learn oil analysis - How to read an oil sample report (video, 2018)
Three common contaminants and the oil analysis tests that can detect them
H Adeni - Testing lubricants and its significance
Koehlerinstrument - Test methods for lubricating oils
Laboratory test method codes and sample sizes
Savant - Laboratory services
Sample report with explanations
TESTOIL - Sample reports
Key oil analysis metrics

Oil analysis reports also frequently lack important test information relating to the machine application and the type of oil, which is essential for proper interpretation. Other common challenges include:
* The same test package is used for different types of machines.
* The individual reading the oil analysis report lacks the appropriate knowledge/understanding.
* The laboratory analyst has no knowledge of the basics of machinery lubrication and tribology.
* The oil analysis report is received several months after oil sampling.
* The lab does not follow strict procedures as per ASTM/ISO standards.
* There is no quality assurance for meeting the required standards.
* The report contains insufficient information to make any decisions.
* No interpretation or recommendation by the oil analysis lab is included in the results.
* Cross-contamination between various oil samples leads to inaccurate results.
Mohammad Naseer Uddin

Advanced test methods

Polaris - Identifying varnish with fluid analysis (1 h webinar, 2021)
Oil analysis tests to detect glycol contamination (short, 2016)
Dr. Neil Canter - Emerging technologies advance traditional condition monitoring techniques (December 2019)
Learn Oil Analysis - Where each element comes from in your machinery (2018)
TESTOIL - Filter debris analysis
TESTOIL - Filter debris analysis report
New advances in wear debris analysis
Michael D. Holloway - How to prevent equipment failures with wear debris analysis (2018)
Microscope (short video)
V4L - CADET Particle analysis demo (short video)
Dangers of small particles and test methods discussed (2018)
Evan Zabawski - Comments on specroscopy
Siqi Sun - Inductively coupled plasma optical emission specroscopy (2020)
TESTOIL - Varnish potential analysis testing (short video, 2020)
Sam Keating - Varnish Identification: Measuring oxidation products through temperature manipulation when particle counting (2019)
Fluitec - Membrane Patch Colorimetry (MPC) test ASTM D7843
EPT - MPC varnish potential testing ASTM D7843 (2016)
EPT - MPC varnish potential testing ASTM D7843 (2:30 video, 2013)
How light affects oil analysis results for varnish potential (2016)
How to detect varnish in turbine oils
Varnish (links)
Oelcheck - Warning values for contaminants, additives and wear
Water and oxidation sensor
TESTOIL - Materials identification analysis
UE - Condition-based approach to lubrication
UE - 3 ways to incorporate ultrasound in lubrication testing
SDT - Ultrasound detector
Monitoring large particles in gear oils
LaserNet Fines (LNF) instrument counts and classifies all particles
Ferrography
Ferrography PQ Index
The value of analytical ferrography as a critical exploratory test
Engineers guide handbook (23 MB, August 2018)

According to Caterpillar, catching a problem before failure occurs results in repair costs that are 5 to 25 percent of the engine's value. Catching a problem after failure occurs leads to repairs that are more than 65 percent of the engine's value.

Today, portable analysers are able to measure many relevant oil parameters at the site with no need to send samples to a laboratory. They can determine oxidation, viscosity, TBN, TAN, water contamination, additive depletion and more.

Root causes of failures, analysis interpretation

Michael W Blanchard - Preparing for a root cause analysis (2021)
Monika Malcolm - Using a root cause analysis to solve plant mysteries and prevent unplanned downtime (2021)
Thomas Brown - Failure analysis tools: choosing the right one for the job (2020)
TESTOIL - Oil analysis report interpretation (webinar, 2020)
TESTOIL - Oil analysis alarm limits (short video, 2020)
Jonathan Trout - Root cause analysis explained (2019)
Andy Page - Interaction between oil analysis and vibration analysis (2018)
Evan Zabawski - Holes in the data (2019)
https://testoil.com/program-management/oil-analysis-alarm-limits/ Wes Cash - Why you should cross-check your oil analysis lab (2017)
Jim Fitch - Be proactive to avoid root cause fault bubbles (2017)
Vibration and oil analysis techniques reveal root cause and severity
Guidelines for using ultrasound and vibration for lubrication (short, 2019)
Extend vibration from mechanical to tribo-mechanical condition monitoring closing the gaps between vibration and oil analyses (2019)
Proven methods for determining the cause of machine failures (2016)
How to diagnose machine failures (2002)
Greg Lee, PRUFTECHNIK Inc. - How to identify the root cause of a misalignment condition (2017)
UE - The 100 failure modes of lubrication and lubrication programs
Acculube - There are 4 main reasons lubes fail (2017)
Root cause analysis (2018)
Quant - Improving equipment reliability through the implementation of Root cause analysis (RCA)
Pinnacle - Root cause analysis
Finding the root causes of oil degradation
Determining the cause of oil degradation
Learn Oil Analysis - What do TAN and TBN mean (2018)
How engines consume oil ... and oil analysis results (2016)
Root cause analysis techniques for the lubrication professional (2002)
Root cause analysis for lubrication failures (2006)
Medical Device Academy - Root cause articles
Root cause analysis, four different investigation tools
Root cause analysis slides
The power of root cause pre-failure analysis (2016)
Root cause analysis training (2017)
Root cause analysis, calculators, tools and assessments (2017)
Reliability-centred maintenance and root cause analysis(2008)
Implementing world-class oil analysis (short video, 2017)
How to interpret oil analysis reports (2016)
Matt Spurlock - Repeating trends in oil analysis reports (2006)
Evan Zabawski - Oil change as a corrective measure?
Learn oil analysis - How to read an oil sample report (video, 2018)
The wrath of unscheduled downtime: Why oil analysis is a wise and effective defense
Making sense of oil analysis results
TESTOIL - Materials identification analysis report
Hi-Pro - What to look for in a dissolved metal analysis (2018)
Oil Analysis: Five Things You Didn't Know
Top 10 oil analysis misperceptions (You can also page through the magazine)
Systematic Oil Analysis Interpretation
Engine oil analysis
In-service fluid analysis, part XL (2018)
Establishing elemental limit values for motor oils
John S. Evans - Wear limits vs. trends (2006)
Set oil analysis limits correctly (2005)
With oil analysis "What you know is what counts" (2005)
Evaluating the source of silicon in oil
Sources of silicon in oil

The presence of silicon in oil is associated with the presence of air-borne dust or dirt. Dirt is not pure silicon, but silicon combines with oxygen (and other elements) to form a family of compounds known as silicates or pure silicon dioxide (also known as silica). Silicon is element 14 in the periodic table and found towards the upper right-hand part of the table. It is a metalloid, which means that it is not wholly a metal or a non-metal but has characteristics of both groups of elements; it is chemically similar to carbon. Silicon is the eighth most common element in the universe but the second most common element in the earth’s crust after oxygen, and has a melting point of 1410˚C.
Unfortunately for the oil analyst, seeing silicon in an oil sample does not always mean that dirt is present; silicon can have many other sources. For a detailed overview of silicon, silicates and sources of silicon please visit the following technical bulletin:

John Evans, Wearcheck - SOS: Sources of silicon (2012)
Sodium in oil
Root causes of sodium and potassium in engine oil

Typical sources of copper within an engine include the wrist-pin bushings, thrust washers, oil pump, governor, valve-train bushings, cam bushings, oil cooler and bearings.

The effects of glycol contamination in engine oils
Learn Oil Analysis - Water or antifreeze (glycol) contamination (2017)
Oil analysis tests to detect glycol contamination (short, 2016)
Identifying root causes of machinery damage with condition monitoring
Hy-Pro - Fluid analysis reference guide
Elemental analysis (2002)
Noria - Elemental analysis (video 2012)
Grant Dawson - Understanding basic oil analysis (video)
Grant Dawson - Oil analysis: Sources of atomic elements
Learn Oil Analysis - Guide to contamination with wear metal elements (2018)
Grant Dawson - Understanding diesel oil analysis reports
Grant Dawson - Spectrochemical metal limits
Adam Cutler, Learn Oil Analysis - Copper, the awkward wear-element that can be high and normal and low and critical (2018)
Understanding automatic transmission oil sample report
Spectro - Fuel dilution testing in the field
Influence of engine oils dilution by fuels on their viscosity, flash point and fire point
Oil filter analysis uncovers hidden problems
Filter element examination
3 ways to analyze an oil filter (short, 2019)
Jeanna Van Rensselar - Filter debris analysis: From aircraft to wind turbines (2018)

Oil analysis reports frequently lack important test information relating to the machine application and the type of oil, which is essential for proper interpretation. Other common challenges include:
* The same test package is used for different types of machines.
* There is no reason to perform oil analysis if the data obtained is not properly understood. With so much information packed into a few pages, reading lab reports can be overwhelming to the untrained eye. Unfortunately, a majority of plant personnel who receive these reports do not understand the basics of how to interpret them.
* The laboratory analyst has no knowledge of the basics of machinery lubrication and tribology.
* The oil analysis report is received several months after oil sampling.
* The lab does not follow strict procedures as per ASTM/ISO standards.
* There is no quality assurance for meeting the required standards.
* The report contains insufficient information to make any decisions.
* No interpretation or recommendation by the oil analysis lab is included in the results.
* Cross-contamination between various oil samples leads to meaningless results.

Grease analysis

Andrea R. Aikin - Condition monitoring of greases (2021)
Grease analysis methods
Grease analysis
Best methods for analysing grease
Grease analysis: Early warning system for failures and proactive maintenance tool

10.2 Oil cleanliness

Jeanna Van Rensselar - Clean lubricant program success (2021)
Scott Howard - 4 sources of contamination in your system (2021)
Hi-Pro - Blogs
Dr Robert M. Gresham - Contamination control (2015)
TESTOIL - Five steps to control lubrication contamination (2020)
Des-Case - Introduction to oil cleanliness (18 Mb, 2020)
Schaeffer - How dirt and water interact with lubricants and their effects on equipment (2019)
How to set oil cleanliness targets (short, 2018)
Steven Lara-Lee Lumley, WearCheck - Keep it clean (2018)
Hi-Pro - How filters are tested (2019)
Noria - Maintaining oil cleanliness standards for better contamination control (short, 2006)
Brendan Casey - How to define and achieve hydraulic fluid cleanliness (2004)
Des-Case - Fundamentals of contamination-control (video, 2018)
Training strategies to control contamination (2017)
Des-Case - Cost saving calculator
FlowEzy - Dirt affects hydraulic performance (2 pages)
Oil target cleanliness calculator (2013)
Harvard - Cleanliness/lubrication
Bosch Rexroth - Hydraulic fluid cleanliness, 5 tips (2013)
Reducing the effects of hydraulic fluids contamination
Des-Case - Fundamentals of lubricant contamination control (2016)
Contamination control is critical
UE - Controlling contamination to control costs
...don't forget contamination
Sources of contaminants
Flow Ezy Filters - How dirt affects hydraulics (short, 2018)
Contamination control is everyone's responsibility (video)
UE - Controlling contamination to control costs
Horizon - Setting contamination flagging limits (2018)
The causes and effects of hydraulic oil contamination (video)
How silt lock can destroy hydraulic valves (2012)
How to mitigate contaminant ingression in hydraulic systems (2017)
How clean is your hydraulic fluid?
Y2K - New oil is dirty
Harvard - Filtering the new oil (short)
Oil Filtration Systems - Filtering brand new oil, why and how (2018)
Cleanliness extends lube, equipment life
Effects of contamination on the pump life (video)
How particle ingression impacts equipment reliability
Rich Wurzbach - Why grease cleanliness should not be overlooked (2018)
Spectro - In-service oil and fuel analysis
Spectro - ICP-OES technology
Monitoring large particles in gear oils
Solid particles
Learn Oil Analysis - Particle counting (2018)
Learn Oil Analysis - Why do particle counters differ in results (2018)
Characterization of particles from in-service lubricants (ASTM)
Dirt is harder than metals in machines
Improve oil cleanliness (short video)
Minimizing the impact of built-in contamination in hydraulic systems
5 tips for setting target cleanliness levels
Bosch Rexroth - Importance of hydraulic oil cleanliness and tips to protect your systems (video)
Chevron ISOCLEAN certified lubricants
Causes and hazards of silt lock
Electrostatic cleaning: Valve stiction problem cured by soft particle removal
How to interpret oil analysis data (2012)
MP FILTRI - Fluid condition handbook (1.2 Mb)
TESTOIL - Hydraulic oil analysis report
Back to Hydraulics

When installing fine-filtration (3 to 10 micron) reservoir breathers, make sure the breather has an internal differential pressure gauge to alert you when the filter is dirty. If your breathers do not have this built in, add pressure and vacuum gauges to the reservoir head space. Then add inspection of these gauges to your pre-PM checks while the machine is in normal operation.

Translucent new oil is visually assumed to be clean but it often contains more contamination than the existing oil being replaced. Typically, new oils delivered to customers are rated 22/21/18 (ISO 1044c Cleanliness Standard – now ISO 4406) and sometimes worse. To eliminate the risk of adding new contaminated oil, the end user is placed in a position of having to filter new oil before it is put into service.

Equipment that is run in an extremely dirty environment, such as in a forge or foundry, needs extra care to avoid contamination. Always try to keep equipment sealed and avoid unnecessary opening of the reservoirs. Install quick disconnects in your tanks and on your fill vessels for filling or topping up hydraulic tanks. All equipment should have mainstream sampling taps installed for uptime or running sampling. This will result in a true indication of the oil condition, avoiding any bottom sampling.
James Ott, Patriot Forge Co.

Why do spool valves in hydraulic systems sometimes stick? In a word: contamination.

In common, garden-variety directional control valves, the radial clearance between the spool and bore ranges between 3 and 13 microns. And in practice, perfectly round and straight bores are difficult to achieve. And so the radial clearance typically varies across the length of the spool. This influences spool friction-but so too does the cleanliness of the oil.

If the clearances between the spool and bore become invaded by hard particles (silt) or soft particles (varnish and sludge), more force is required to move the spool. According to test data from Eaton Hydraulics, if the radial clearances of a one eighth inch spool valve operating at 3,000 PSI silt up, 30 pounds of force is required to move the spool. But if the valve is solenoid operated, the solenoid can only exert 10 pounds of force!

This problem is commonly referred to as 'silt-lock' and can be especially problematic for valves in contaminated systems which are operated infrequently. Furthermore, if a silt-locked valve is operated by an AC solenoid, then the likely outcome is a burnt-out solenoid. This occurs because the silted spool prevents the solenoid plunger from being completely pulled into its coil. And as a result, the coil is exposed to inrush current for as long as it is energized-the heat from which it can't dissipate. This causes the insulation around the coil windings to break down and the coil eventually shorts out.

The good news is preventing valve silt-lock is simple enough. Keep the oil 'clean, cool and dry'. The 'clean' i.e. adequate filtration combined with the elimination of particulate ingression points will take care of the hard particles. The 'cool and dry' i.e. not letting the system run too hot and preventing the ingression of and removing water will eliminate the formation of soft particles, such as varnish and sludge.

There are generally only two conditions that necessitate changing the oil in a hydraulic system:
1. Base oil degradation
2. Additive depletion

Contaminants of the hydraulic fluid such as hard and soft particles and water can be removed from the oil and therefore don't mandate an oil change.

Techniques for flushing hydraulic systems vary in cost and complexity. Before I discuss some of these methods, let's first distinguish between flushing the fluid and flushing the system.

The objective of flushing the OIL is to eliminate contaminants such as particles and water.

This is usually accomplished using a filter cart or by diverting system flow through an external fluid-conditioning rig.

The objective of flushing the SYSTEM is to eliminate sludge, varnish, debris and contaminated or degraded fluid from conductor walls and other internal surfaces, and system dead spots.

Reasons for performing a SYSTEM flush include:

1. Fluid degradation - resulting in sludge, varnish or microbial deposits.
2. Major failure - combined with filter overload disperses debris throughout the system.
3. New or overhauled equipment - to purge 'built-in' debris.

Common methods for flushing hydraulic systems include:

* Double oil and filter change.
* Mechanical cleaning.
* Power flushing.

The technique or combination of techniques employed will depend on the type of system and its size, your reliability objectives for the equipment and the reason for the flush.

Double oil and filter change
This technique involves an initial oil drain and filter change, which expells a large percentage of contaminants and degraded fluid. The system is then filled to the minimum level required and the fluid circulated until operating temperature is reached and the fluid has been turned over at least five times.

The oil is drained and the filters changed a second time. An appropriate oil analysis test should be performed to determine the success of the flush.

To maximize the effectiveness of this technique, the system should be drained as thoroughly as possible and the reservoir mechanically cleaned.

Mechanical cleaning
Although not technically a flushing technique, the selective use of mechanical cleaning may be incorporated in the flushing strategy.

This can involve the use of a pneumatic projectile gun to clean pipes, tubes and hoses, and disassembly of the reservoir and other components for cleaning using brushes and solvents.

Mechanical cleaning is labour intensive and therefore costly. It carries with it reliability risks associated with opening the hydraulic system and intervention by 'human agents'.

Power flushing
Power flushing involves the use of a purpose-built rig to circulate a low viscosity fluid at high velocities to create turbulent flow conditions (Reynolds number > 2000).

The flushing rig is typically equipped with a pump that has a flow rate several times that of system's normal flow, directional valves, accumulators, fluid heater and chiller and of course, a bank of filters.

The directional valves enable the flushing direction to be changed, the accumulators enable pulsating flow conditions and the heater and chiller enable the fluid temperature to be increased or decreased, all of which can assist in the dislodgment of contaminants.

Analysis of the flushing fluid is performed regularly during the flushing operation to determine the point at which the system has been satisfactorily cleaned.

What about components?
The question of how to deal with system components arises when contemplating a hydraulic system flush. Plumbing should be flushed first in isolation from pumps, valves and actuators. Once the conductors have been flushed clean, valves and actuators can be gradually included in the flushing circuit.

The decision to disassemble and mechanically clean components will depend on the type of equipment, your reliability objectives and the reason for the flush.

With the exception of new or overhauled equipment, the need to flush a hydraulic system generally represents a failure of maintenance.

If you follow an effective proactive maintenance program like the one I outline in 'Insider Secrets to Hydraulics', it's likely you'll never need to flush!
Brendan Casey

Particle counting, purifying oil, preventing contamination

Understanding ISO codes (2021)
SAIT - Particulate detection in lubricating oil (2009)
Whyps - Cleanliness monitoring of hydraulic systems
Parker - Guide to contamination standards
Spectro - Particle measurement techniques
How to get the most from tour particle counter (2018)
Particle counting - oil analysis 101
Devin Jarrett - Particle counts: what they mean and how to use them (2019)
Beckman Coulter - Importance of particle counters (2017)
Particles: friend or foe? Understanding the value of particles in oil analysis (2012)
Hydraulic oil contamination (NAS, ISO)
Oil cleanliness codes
ISO 4406 Cleanliness Code
How important is the ISO Cleanliness Code in oil analysis? (2012)
ISO 4406: What do those numbers mean in the ISO Cleanliness Codes?
ISO Cleanliness Codes (video)
Des-Case - ISO Cleanliness
Elevated particle count - what now?
Value of particle counting in oil analysis
Particle counters
A much closer look at particle contamination
MP Filtri - Continuous contamination monitoring
Spectro - Detection of abnormal wear particles in hydraulic fluids via electromagnetic sensor and particle imaging technologies (2018)
Advantages of having an on-site particle counters (short video)
Parker - Oil purifier
Dr Robert M. Gresham - Contamination control (2015)
Contamination control strategies for turbomachinery (2016)
Synthetics, contamination control and oil analysis team up
When fluid that is cleaner than ISO 14/12/9 is required...
Valve stiction problem cured by soft particle removal (electrostatic liquid cleaner)
SWEPCO 728 In-service system cleaner
Gearbox contamination control - Breathers
How to improve desiccant breather life (short video)
Filler-breather adapter simplifies hookups (2017)
Des-Case - Connected breathers (2018)
TTI - How to make the most of your desiccant breathers (2020)
Des-Case - How to select breathers (2018)
Des-Case - Desiccant breathers
TTI - Desiccant breathers (2020)
TTI - How to get more value from your desiccant breathers
Jonathan Trout - Desiccant breather buyers guide (2019)
Jonathan Trout - Desiccant breather buyers guide (alternative address, 2019)

General Motors concluded that, "Controlling particles in the 3 micron to 10 micron range had the greatest impact on wear rates and that engine wear rates correlated directly to the dust concentration levels in the sump."

Some additives can interfere with the particle count. Perhaps the biggest offender is the silicone defoamant, which is not dissolved in the fluid but rather suspended as microglobules in the 5 to 10-micron range.

One simple way to track the success of lubrication best practices in contamination control is by charting filter changes on equipment due to plugged filters. Before implementing improved contamination exclusion practices, we were getting at least one plugged filter per week on eight separate lube systems. A year after implementing best practices, we may get a plugged filter every three months. This has cut downtime costs, off-quality time, as well as filter and oil costs.
Brian Lees, Norske Canada

Particle Volume Indexing (PVI))
Consider the particle sizes as well as particle size distribution that different wear mechanisms can generate. In many instances, particle sizes start small and grow progressively larger as a wear problem increases in severity.
ISO 4406 particle counting is an excellent tool for determining oil cleanliness but particle count data itself also allows us to quantify particles into different size ranges. This quantification is often referred to as the particle size distribution. Particle size distribution is an important factor when trying to assess the development of an abnormal wear situation.
PVI is a non-standard index number, originally developed by a major earthmoving OEM (Original Equipment Manufacturer). PVI estimates the total volume of all the particles in the oil sample based on the particle count data obtained in all eight channels of the particle counter from four to 100 microns. PVI can be a useful tool for identifying and evaluating shifts in the particle count distribution that could indicate an abnormal wear situation developing. The value of PVI lies in its ability to express all eight channels of the particle counter as a single number which makes spotting changes in the particle size distribution easier.
Steven Lara Lee Lumley, Wearcheck, South Africa (stevenl@wearcheck.co.za)

Filtration, filters

Be sure to monitor your filter change interval. Premature plugging is usually a sign of a problem that merits further investigation. This may be caused by airborne dust from nearby construction or a prolonged dry spell raising atmospheric dust levels. Whatever the source of dirt, the root cause should be investigated, and the seals or breathers may need to be serviced or upgraded. In certain cases, the problem may be associated with a change in the performance of the filter from your supplier. Extremely long filter life is as much of a concern as too short of a life.

Have you seen a spike in particle counts for a stable circulating oil system where no oil has been added or lost? Check to see if the oil filter was changed just prior to the sample date. It's not uncommon for a spike in particle counts to occur after changing filters due to the system "disturbance." Therefore, don't be too zealous in changing filter elements purely on a calendar basis. Take advantage of their operating life and only change them when they have reached load capacity or been in the system for the recommended service life.

Ivan N. Sheffield - Cleanliness programmes are key to keeping oil and hydraulic fluids at their best (2021)
John Fleming - Selecting the appropriate filtration system contributes to longer service life (2021)
TESTOIL - An in-depth look at filtration (webinar, 2021)
Alan Hitchcox - Understanding filtration specifications (2019)
Curt Rausch - Which hydraulic filters are most effective (2002)
Bennett Fitch - The effects of water contamination on oil filters (2018)
Steffen D. Nyman - How to verify oil filtration efficiency (2018)
Hi-Pro - Servo valve failures: A video case study (2019)
Hi-Pro - Blogs
Bill Novak - Five must-knows for successful hydraulic filter sizing (2019
LubriSource - Understanding oil filtration (brief, 2019)
Jim Fitch - Managing the costs of lubricant filtration (2005)
When should oil be filtered?
Taher Salah et al, Hydraulics & Pneumatics - Integrated monitoring and filtration in a steel mill (2018)
Des-Case - Filter new oil
TESTOIL - Fluid filtration and the importance of cleanliness (webinar)
Keeping fluid clean in the reservoir (2017)
Some interesting blogs in English - Click on 2013 in Blog archive, scroll down near the bottom, 3 June 2013: High speed oil flushing and filtration
C.C.Jensen - Off-line fine filter
Hi-Pro - Benefits of offline filtration (2018)
C.C.Jensen - Offline filters for gearboxes
C.C.Jensen case study: Conveyor belts gear box (one page, 2009)
Harvard - Why supplemental filters?
RPS - Filter carts
Macpherson curve graph
Macpherson curve: clean oil = 70% gearbox life extension
C.C.Jensen - How to use offline filters to rescue dirty gearboxes
Selecting the right oil filter
Dustin Flynn - Dynamic filter efficiency (2021)
Jeremy Wright - Understanding filter efficiency and Beta Ratios (2008)
Understanding oil filter ratings
C.C.Jensen - Oil filtration
C.C.Jensen - Tools to verify oil filtration efficiencies
How to evaluate oil filters (video)
Oil filters (video)
MP Filtri - Filters (just 2 pages, 2018)
Changes in filtration and contamination - switching directions for the filtration industry
Parker Racor - By-pass oil filtration of engine oil
By-pass oil filtration
ROI with kidney loop by-pas filtration
How to select the right filtration skid for offline kidney-loop oil filtration (2018)
High viscosity gear oil filtering (short video)
Reducing wear particle generation (filtering and using PAG)
12 guidelines for using oil filters (2012)
Hi-Pro - Oil filter elements and media types (2018)
Noria - Dirt-holding capacity of filters (short video, 2018)

For the same size, microglass and fibreglass filters hold more dirt than cellulose filter media types.

One mining company was replacing a 460 litre per minute piston pump and a radial hydraulic motor approximately three times per year. The solution was to install ten micron bi-directional filters in the ‘A’ and ‘B’ lines of the closed loop hydrostatic system lines. After seven years the pump and motor were still working, performing without a problem.

One company wanted to replace their 30-solenoid operated directional control valves with another make as they were replacing the solenoids daily. The standing order for solenoids was 125 per month. Once the oil was filtered the company had no more problems. That was the worst incident that was encountered. Solenoid failures are generally two to three per month, once correct filtration is applied solenoid failures almost cease.
Garnett Cross

Select the right gearbox piping
When retrofitting gearboxes for service and filtering, consider using stainless-steel piping instead of black iron piping. After a rather short period of time, the inside of the black piping may begin rusting and flaking off into the gearboxes, producing false test results. This is more predominant in high humidity and frequent washdown areas.
Jeffery May, Harmony Corp.

Choosing the oil filter location (2017)
Fundamentals of filters - Select page 18
Matching oil filtration to machine requirements
C.C.Jensen - Oil filters (video)
Hy-Pro - Dynamic Filter Efficiency testing method (2016)
Hy-Pro - Problems with C.C.Jensen cellulose media filters
High viscosity gear oil filtering
PALL - Oil filters and purifiers
Y2K - Removing moisture and particulate contamination
Y2K - All filters are not created equal
Harvard - Oil filter carts (2018)
Oil Filtration Systems (2020)
Additives not removed by filters (2013)

Maintenance tip: Equipment optimisation through modification

More than 75% of all problems in fluid systems can be traced back to contaminated oil. Therefore, proper lubrication goes beyond choosing the correct lubricant; it includes keeping the lubricant free of contaminants and monitoring oil cleanliness is the most important factor in preventing system failures.
You might have to modify the equipment so it remains sealed during all phases of normal operation—including routine maintenance, such as level checks and oil changes. This can be achieved by retrofitting the drain and fill/breather ports with modification kits that permit multiple access points to the equipment without opening the sump to the environment. Modifications should be designed in a way to help you:
- Top up oil
- Check oil level
- Take oil samples
- Drain/fill oil
- Kidney loop oil filtering

Advice

When replacing top-suspended spin-on or threaded canister-type filters, fill them with fresh oil before installation. This will reduce the amount of time that the engine or machinery undergoes dry start-up by having that extra available amount of oil available. In some cases, it could also prevent filter damage when a gush of high-pressure fluid hits a dry element.

From Brendan Casey:

"Brendan, your book 'Insider Secrets to Hydraulics' motivated me to build a small, kidney loop filter cart comprising a 145 micron screen, pump, water absorbing filter and final 3 micron filter (Donaldson P550275, P565062 and P551550 respectively). A second-hand 3 GPM pump and motor drive the system.

The limiting factor is inlet vacuum at the pump which I limit to less than 5 PSI via a pressure relief valve at the pump outlet which relieves back to the intake side of the inlet filter. That routing was chosen to provide rough filtration and more heat exchange surface for the oil being recirculated within the pump.

With cold hydraulic oil this gets me a throughput of around 1 GPM which I run for several hours to get several full passes. All very modest, but a real money saver. The alternative - annual oil changes - would cost around $450 at today's $15/gallon prices. The total cost of my self-made cart was less than that so it paid for itself in the first year. I suppose I should still change the oil every three years or so to maintain the additives and all. Even at that rate the cart will have reduced my oil cost to one third of what it would have been. Rather satisfactory."

Brendan Casey comments: Is this filter cart design technically perfect? Probably not. Is it effective at cleaning and drying the oil? Almost certainly. Sure, this member needs to get a bit more sophisticated and do regular oil analysis - to know for sure when the oil's additives and/or oxidative life have been used up.

Advice

High Velocity Oil Flushing is an essential process to ensure optimal reliability of critical components within hydraulic systems and the lube oil systems of rotating equipment.
Flushing may often be required when the system is new or during subsequent service, particularly after repairs, if significant contamination has occurred. Large systems assembled on site frequently incorporate components treated with temporary corrosion protectives. Unless such materials are removed prior to filling the system with a clean hydraulic fluid, they will gradually dissolve in the working fluid and may detract from its performance in several respects, e.g. by promoting emulsification.
If flushing is required, it is preferable to utilize the grade to be used in service or a lower viscosity grade of similar composition. Critical components (valves, hydraulic pumps and motors) should preferably be isolated or by-passed during the flushing operation to avoid harmful accumulations of particulate contaminants, thus defeating the purpose of the treatment. A minimum charge of flushing oil should suffice, this being circulated through the system and adequately dimensioned supplementary filter(s) by a suitable external pump. Filters should be checked periodically and flushing continued until particle counts on the fluid returning to the filters decrease to a satisfactory level.
Hydraulic Fluids
Some oil companies offer a mineral oil-based flushing oil.
Otherwise, diesel fuel will completely mix with the mineral oil lube in use. It may be a better cleaning agent than the lube oil and will not have any compatibility issues.The only issue is that any residual diesel fuel left in the sump after the flush will dilute and lower the viscosity of the new charge of lube oil.
The chemical cleaning solution or agent is likely the best cleaning option, but you must be sure to get all of the cleaning solution out of the sump. This may require a fill and drain (flush) with the new lube oil to be used, then a final fill with the new lube oil to be used in the operating equipment. Any remaining cleaning solution may cause issues with emulsification of water or foaming and aeration. Also, make sure that the chemical solution is compatible with any seals and paints in the sump. Temperature and flow rates also affect flushing effectiveness.
Bob Scott, Noria

Flushing

Advice for flushing sumps (short, 2012)
Factors to consider before an oil flush (short, 2017)
Automatic transmission flushes (video)
Flushing methods (Solving recurring oxidation problems)
11 simple steps for flushing a hydraulic system
Pulsating hot oil flushing technology
Some interesting blogs in English - Click on 2013 in Blog archive, scroll down near the bottom, 3 June 2013: High speed oil flushing and filtration
Four types of oil flushes
How to verify system cleanliness after an oil flush (2017)
Alternatives to lubricant flushing

Water contamination

Noria: The presence of water in most lubricants (synthetic or mineral) can cause the progression of oxidation to increase tenfold, resulting in premature aging of the oil, especially in the presence of catalytic metals such as copper, lead and tin. In addition, certain types of synthetic oils like phosphate esters and dibasic esters are known to react with water, which leads to the destruction of the base stock and the formation of acids.
It is not just the base oil that can be affected by moisture contamination. Certain additives such as sulfurous anti-wear (AW) and extreme-pressure (EP) additives as well as phenolic antioxidants are readily hydrolyzed by water, causing both additive mortality and the formation of acidic by-products. These acidic by-products can produce corrosive wear, particularly in components containing soft metals like Babbitt, which is used with journal bearings, as well as bronze and brass components. Other additives, including demulsifying agents, dispersants, detergents and rust inhibitors, can be washed away by excessive moisture. This results in sludge and sediment build-up, filter plugging and poor oil/water demulsibility.

In turbine oils, moisture content could reach 180 ppm before the oil turns cloudy. So the easiest way to check for water is visual, done at room temperature. At 250 ppm, the lubricant is still translucent but hazy. At 500 ppm, it is hazy and opaque. At that level, by decreasing water concentration, lubricant's service life extends almost twice for every 120 ppm water eliminated. There is also the crackle test: if no crackling takes place after placing a drop of oil for a few seconds on a small metal pan at 135 °C, no free or emulsified water is present. If some 0,5 mm bubbles are produced aprox. 500-1000 ppm water is present. For moisture content of more than 2000 ppm, bubbles grow to 4 mm. This method does not measure chemically dissolved water. Other methods would be calcium hydride test and capacitance change of the sample or FTIR or Karl Fischer.
Denisa Ivana

Drew Troyer - Establishing moisture contamination targets for hydraulic systems (2004)
Ken Kaihlanen, Oil Filtration Systems - Water contamination in hydraulic and lubrication oils (2020)
Next Generation Filtration Systems - Conserver oil purification unit, failures due to water contamination including hydrogen embrittlement (2020)
Mark Barnes, Des-Case - When water and oil mix, assets suffer (2020)
Humidity saturation limits of lubricating oils (2012)
Why water and oil don’t mix - and what to do about it (5.5 Mb)
BioKem - Moisture could be your No. 1 lube oil problem
How water causes bearing failure
Oil and water shouldn't mix
Learn Oil Analysis - Water in oil, how to prevent it and how to fix it (2018)
LE - Water contamination
Understanding oil's saturation point
Humidity saturation limits of hydraulic and lubrication fluids
Water-related damage to rolling element bearings (video)
Case study: The power of water (2018)
Impact of water on EHL film thickness of lubricating greases in rolling point contacts
Impact of water on EHL film thickness of lubricating greases in rolling point contacts (full article)
Water in oil contamination
Water in oil
Water in oil
Strategies to achieve and sustain dry oil
How should I remove water from my oil reservoir?
Best ways to remove water from oil (2012)
Removing water contamination from oil
C.C.Jensen - Winning the war on water contamination (2019)
How to determine water in oil (brief)
Alejandro Meza - Modern methods for monitoring water contamination (2019)
How to measure water in oil (2002)
Best ways to test for water in oil
Karl Fischer methods
Arizona Instrument - Relative humidity test
Guide to measuring water in oil
Spectro FluidScan alternative to Karl Fischer (2014)
Water in oil: How does the laboratory determine this?
HY-PRO - Removing dirt and water using vacuum dehydrator

Water in hydraulic fluid:
- Depletes some additives and reacts with others to form corrosive by-products which attack some metals.
- Reduces lubricant film-strength, which leaves critical surfaces vulnerable to wear and corrosion.
- Reduces filterability and clogs filters.
- Reduces the oils ability to release air.
- Increases the likelihood of cavitation occurring.

It's always wise to control water contamination at the lowest levels that can reasonably be achieved, but certainly below the oil's saturation point at operating temperature.

Methods for removing free (unstable suspension) and emulsified (stable suspension) water include:

1. polymeric filters;
2. vacuum distillation; and
3. head space dehumidification.

Polymeric filters - These look like conventional particulate filters, however the media is impregnated with a super-absorbent polymer.

Water causes the polymer to swell, which traps the water within the media. Polymeric filters are best suited for removing small volumes of water and/or maintaining water contamination within pre-determined limits.

Vacuum distillation - This technique employs a combination of heat and vacuum. At 25 inches of mercury, water boils at 56 °C. This enables water to be removed at a temperature that does not damage the oil or its additives.

Head space dehumidification - This method involves circulating and drying the air from the reservoir head space. Water in the oil migrates to the dry air in the head space and is eventually removed by the dehumidifier.

Vacuum distillation and head space dehumidification also remove dissolved water.

Like all other forms of contamination, preventing water ingress is ten times cheaper than removing it from the oil.
Brendan Casey

SKF recommends a conservative 200 ppm limit of water content. This can be achieved with desiccant breathers and proper water removal techniques (vacuum separation, centrifugal separation). Most circulating systems have tanks to allow some standing time to promote separation.

Some greases and oils can carry as much as six percent water when mobile. Water separates readily at a standstill and displaces oil on metal surfaces - attacking metal surfaces directly. Avoid standstills with water in the system if possible.

A good way to get an estimate of the concentration of water in oil is to use the calcium hydride method. There are different suppliers and variations on how to do this. The basic concept is that you put some oil and kerosene into a vessel. The instrument that you buy will have this vessel as a part of it. A calcium hydride capsule is placed in with the kerosene and oil. The vessel is then sealed and agitated.

In humid environments, condensate can form in rolling-element bearings and cause corrosion, leading to a reduction in bearing life. The condensed moisture's effect can be reduced by carefully choosing the grease lubricant. Greases thickened with sodium soap will absorb (emulsify) large quantities of water but may soften it to such an extent that the grease flows out of the bearing. Lithium soap greases do not emulsify water but with suitable additives can provide good protection against corrosion.

Although grease can absorb large quantities of water, separation occurs due to pressure and shear, leading to free water. This does not have an impact on the film thickness under fully flooded EHL conditions. However, water does have an effect on the film thickness under starved conditions where the differences are related to the change in oil bleed. In the presence of water, an increase in oil bleed was found for lithium, lithium complex and polyurea grease. These greases showed a reduction in the levels of starvation and, therefore, thicker films. Water contamination led to lower oil bleed for calcium sulphonate complex greases, which led to an increase in starvation, and therefore, thinner films compared to their uncontaminated counterparts.

1. Educate maintenance staff to avoid direct jetting of water at ingression points such as shaft seals and breathers, etc.
2. If water spray is inevitable, use passive shields and deflectors to avoid direct water spray on shafts, dipsticks, fill-caps, breathers, etc.
3. Use high-performance seals that suffer less wear and offer better protection against contaminants.
4. Regularly inspect and maintain gaskets on fill-caps, hatches, etc.
5. Replace dipsticks with level indicators.
6. Keep hatches closed tight.
7. Replace a basic vent breather with a desiccant breather, which dehydrates incoming air, or an expansion chamber, which allows the system to breathe without ingesting external air.
Noria

Maintenance strategies - reactive, preventive, predictive and proactive

Combining effective failure analysis with a good predictive maintenance program usually results in huge benefits. Depending on the type of facility, it can not only reduce maintenance costs by 20-30 percent but also increase production by similar values. However, it does require a cultural change.

3 Easy steps for proactive maintenance (short video, 2018)
Devin Jarrett - Getting started on the path to lubrication excellence (2018)
Jack Weeks - Proactive vs. Reactive hydraulic maintenance (2018)
Matthew Adams - How controlling three contaminants significantly reduces machine failures (2018)
Alejandro Erives - Understanding failure (45 minute video, 2018)
5 ways to transition to proactive maintenance practices (2018)
Securing your future with proactive maintenance
Making the transition to proactive maintenance (2016)
John Day, 1997 - Proactive maintenance (slides)
Abnormality reporting key proactive maintenance
Keys for a proactive maintenance approach (short 2018)
Why proactive maintenance is key for a world-class lubrication program
Proactive maintenance at Weyerhaeuser - putting the theory to test
Day in the life of a proactive maintenance planner
Quant - Industrial maintenance today and future trends (Proactive)
Why proactive maintenance is key for a world-class lubrication program
Preemptive contamination control (page 42)

The cost of a reactive maintenance program can be up to 10 times that of a proactive approach.

Data proliferation: There will be a mountain of data types with the advent of holistic CM and the varied techniques and disciplines utilized. Powerful intelligent agents (IA) will be needed. That means that manual evaluation would be almost impossible and add unnecessary risk of missing subtle patterns.

Reliability Centred Maintenance (RCM) was originally called On-condition Maintenance, a term coined by the commercial airline industry. Three surprising discoveries were made:
(1) Scheduled overhaul has little effect on the overall reliability of a complex item unless the item has a dominant failure mode.
(2) There are many items for which there is not an effective form of scheduled maintenance.
(3) Preventive maintenance actually increased the rate of failure in some cases. Scheduled maintenance tends to increase breakdowns, and this can only be because it is doing harm by disturbing a relatively satisfactory state of affairs.

Management, maintenance management, Total Productive Maintenance

The new ICML 55.1 standards requirements book($175), represents a consensus of the worldwide machine lubrication community pertaining to well-established best practices to optimize your plant's lubrication management. Adoption of the ICML 55.1 requirements will help your company efficiently manage physical lubrication and asset policies, strategies and plans. Lubrication management systems for mechanical assets assure that your objectives can be achieved consistently and substantially.

Maintenance glossary
Procedure-based maintenance (2018)
Henk van Vugt - Journey to world-class maintenance (49 minute video, 2018)
Prioritize maintenance, repair and operations (MRO) (short, 2018)
5 Tips for keeping machines in good working condition (very short, 2018)
Download R. Keith Mobley’s Reflections on excellence
Terrence O’Hanlon - All leadership comes down to this: changing people’s behavior (2019)
5 ways to drive innovation in manufacturing (2018)
How to manage and benefit from change
Jim Fitch - The importance of sustainability for transformational change (2018)
A tactical approach for improvement
An effective way to drive improvement
Executing a continuous improvement plan
Partnering for continuous improvement
Create, implement improvements daily
The road to prescriptive maintenance
Strategies to manage asset performance (2018)
8 steps to better Kaizen results
4 common maintenance problems (2016)
Noria case studies
Bryan Christiansen - Lean maintenance (2019)
Applying Lean Six Sigma methodology
Jonathan Trout - Six Sigma: A comprehensive overview (2019)
Applying Lean Six Sigma principles to lubrication
Using lean principles to make your plant cleaner and more efficient (2018)
The lean manufacturing techniques
Secrets to becoming a world-class PM facility
Ryan Chan - How to improve your PM programme in 10 steps (2019)
Communicate to build world-class culture
Remedies for a bad maintenance culture (2015)
Greg Perry - How to change your maintenance culture (2017)
Christopher Brokopp - How to change your lubrication culture (2017)
Employ 'Standard work' in maintenance
Signs you are in the real world of maintenance
Three pillars of world-class maintenance
5 tips for greater workplace efficiency
Maintenance: Time and staff optimization analysis (2016)
Best practices for maintenance supervisors
2 keys for organisational effectiveness
Measuring the financial impact of a successful lubrication program (2016)
Autonomous maintenance: 5 steps to successful implementation
5 corrective and preventive maintenance levels you need to learn about
The power of maintenance KPIs (2017)
9 principles of modern maintenance (2018)
Key factors to a better industrial management
How to define world-class maintenance (2018)
How to implement effective maintenance planning and scheduling
Inspection 2.0: The cornerstone of world-class Total Productive Maintenance (TPM) (2016)
Achieving total productive maintenance without supervisors
Total Productive Maintenance (TPM), India - Articles
RELIABLE PLANT videos

Reliability, RCM

Nick Jize - The reliability culture: Six common culprits (2020)
Drew Troyer - Rationalizing your reliability investments (2020)
FLUKE - Condition-based maintenance tools and P-F curve (webinar slides, 2020)
Brian Harrison - Connected reliability 101: A roadmap to predictive maintenance (30 minute video, 2019)
Reliability web - videos
Alan Luedeking - A holistic approach to reliability-centered maintenance (Rcm) relies on good asset condition management (ACM) (2016)
John Reeve - Demanding excellence from your asset management system (2019)
FLUKE - Accelerating the reliability journey (2019)
Bryan Christiansen - 5 obstacles to implementing rcm and how to overcome them (2019)
Jonathan Trout - How to implement reliability-centered maintenance (2019)
RCM, PMO and FMEA: What is the difference? (43' video, 2018)
Connected Reliability (2019)
Nick Jize - The reliability culture: six common culprits (2019)
Rajiv Anand, Michael K. Andrews, Mary Bunzel, Sandra DiMatteo, Blair Fraser, Rendela Wenzel, Terrence O’Hanlon - A new digitalization strategy framework to advance reliability and asset management (2019)
Kevin Price - Plant reliability in the post-digital era (2020)
Natalie Blythe - Creating a culture of lubrication excellence and reliability-centered maintenance at the Ingredion plant in Winston-Salem, North Carolina (2019)
Dale Emanuel and Jorge Mastellari - Critical factors to achieve world-class manufacturing reliability (2019)
UE - P-F curve and reliability centred maintenance
Loctite - Make reliability-centered maintenance a top priority
UE - Understanding the P-F curve and its impact on reliability centred maintenance
What a maintenance reliability program should look like
C.C.Jensen - Proper oil maintenance and the price of reliability vs the cost of reliability (2018)
Stephen Steen - Why online oil quality monitoring is a best practice for reliability programs
Reliability case studies
UE - How proper lubrication can enhance your plant's reliability (2017)
Machine modifications that increase reliability
The Internet of reliability series (videos 2018)
Reliability web - Articles
Wikipedia - Reliability-centered maintenance (RCM)
RELIABLE PLANT videos
Origins of Reliability centered maintenance
Nancy Regan - Lessons from a master: The most valuable RCM business and life lessons John Moubray (1949-2004) taught me (50' video, 2017)

The most influential mentor of my career died on January 15, 2004. Thirteen years later, John Moubray’s wisdom continues to serve me. If you have anything to do with Reliability Centered Maintenance (RCM), then you know who John Moubray was. No matter what your perspective is on RCM2, there’s no denying that John was a giant in the RCM world; he was a fierce proponent of the RCM philosophy designed by the original architects, Nowlan and Heap. He trained his network members to be responsible custodians. John said it best when he affirmed: we are here to promulgate the principles we believe to be best practice and in so doing make the world a safer place for all who live in it. In 1997, by luck (or Providence), I stumbled upon Aladon LLC and the RCM2 process, and thus began my journey into RCM. John Moubray became my mentor. This presentation summarizes the most important RCM lessons John delivered about the process he described as “majestic.” However, a keen entrepreneur, John’s wit and wisdom extended beyond RCM. This presentation also features his insights on business and life that are just as relevant (if not more relevant) today as they were nearly twenty years ago. Ever-grateful for the treasure of John Moubray’s philosophy, the presentation ends with the most valuable advice he ever gave me – advice that applies to everyone (and has nothing to do with RCM!). Nearly two decades later, I finally get it!
Nancy Regan

Reliability resolutions for improving operations and maintenance:

1. We will provide leadership and communication about organisational changes.
2. We will train in best practices and provide on demand refreshers.
3. We will expand our maintenance planning into day-to-day tasks.
4. We will keep our schedule updated 4 weeks in advance.
5. We will solve problems and eliminate reoccurring failures.
6. We will capture both useful data and site knowledge.
7. We will let the equipment talk to us via the condition based tools.

Maintenance/Industry 4.0, Internet of things (IoT), AI, CMMS

Industry 4.0 is the fourth revolution in manufacturing. We are in the midst of a significant transformation of global industry that is blurring the boundaries between the physical and digital worlds. Technology is rapidly changing the businesses we are in, with this shift being reflected in new business models.

With the implementation of computerized maintenance management systems (CMMS), the manufacturing industry became incredibly more efficient. A CMMS tracks system maintenance, inspections and breakdowns, making system disruptions smaller and even obsolete. Instead of manually tracking problems or changes on a piece of paper, a CMMS handles all of this remotely, increasing productivity. The benefits include fewer repairs, lower maintenance costs, a streamlined workforce, and historical data and trend reports.

CMMS technology also connects devices remotely, allowing them to "talk" to each other. Often referred to as the Internet of Things (IoT), it connects factories to the Internet, enabling automation and remote monitoring. Rather than a manual check, the IoT allows systems to be connected to each other and essentially monitor each other's process.

With this connection, plants can easily collect and aggregate big data, or a mass of information concerning their systems. This information can be measured and analysed to increase productivity and efficiency. The IoT helps manufacturers work better by getting products to consumers faster.

Data when you need it: A guide to ensuring your reliability experts have the right information (2020)
Sheila Kennedy - Condition monitoring – take it with you (2020)
Michael Mendoza - 8 ways the IoT can modernize your field service and fleet management team (2020)
William Jacobyansky - Why you need good maintenance procedures (2020)
Eric Holzer - Supercharging oil analysis with AI (short, 2018)
Katie Kellenberger - Europe still sceptical of Industry 4.0 (12 February 2019)
Eitan Vesely and Deddy Lavid - The 7 guiding principles of a Maintenance 4.0 strategy (2019)
Cary Forgeron - Why machine learning and AI are the future of oil analysis (2019)
Milt Olsen - Machine condition monitoring and the industrial internet of things (42 minute video, 2018)
Rajiv Anand, Michael K. Andrews, Mary Bunzel, Sandra DiMatteo, Blair Fraser, Rendela Wenzel, Terrence O’Hanlon - A new digitalization strategy framework to advance reliability and asset management (2019)
Kevin Price - Plant reliability in the post-digital era (2020)
Jim Fitch - How IIoT is changing condition monitoring (2019)
Marco Vieira - Move to IoT-based machine condition monitoring (2018)
Michael Brooks - Improving asset performance with machine learning (2018)
Understanding IoT platforms
Dispelling Industry 4.0 myths (2019)
The essential guide: What is Industry 4.0? (2018)
Maintenance 4.0
Mobility Work - Next-gen maintenance in the context of industry 4.0 and IOT (2018)
Mobility Work - 5 keys to choose your CMMS software (2018)
Advantages of plant digitalization (short, 2018)
IoT and Maintenance 4.0
Charles Rathmann - The next industrial revolution: transformational IoT (2018)
Dr. David Almagor - Will IIOT technologies replace factory maintenance workers? (2018)
National Instruments - Online asset monitoring software (2018)
Stephen Steen - Why online oil quality monitoring is a best practice for reliability programs
UE - How can a remote monitoring platform revamp your PdM process? (2017)
Don’t let infected fluids afflict your operations (page 28)
IIoT for predictive maintenance applications at Duke Energy (2018)
Smart automation tools unlock competitive advantage in lubricant technical service (Must read article, 2017)
Why you should try smart maintenance (2018)
Noah Bethel - Hybrid analytics: the value of machine and human supervision (2018)
UE - How ultrasonic sensors and artificial intelligence improve condition monitoring (2017)
CMMS - How to plan your maintenance (2016)
Peak condition: How to get the most out of your CMMS/EAM investments (2018)
Successful implementation of computerised maintenance management system (CMMS)
Chris McNamara, Smart Industry - IIoT for predictive maintenance? (2018)
Eric Morgan - The technology for better preventive maintenance procedures (2019)
RELIABLE PLANT videos

Executives and managers who believe that Big Data without data analysts is capable of preventing future issues and solving problems as they occur are placing their company and its assets at risk. Over-reliance on the machines in an unsupervised data interpretation environment can have a deleterious impact on plant reliability and the ever-present bottom line.
That is the whole point of hybrid analytics—allowing the machines to crunch the data, which is then leveraged by the supervision of a data analyst whose skills and technological expertise add significantly to machine learning.
Noah Bethel

Lubrication practices, lubrication excellence

Training, education, skills

Michael D. Holloway - Which professional lubrication certification is right for you? (2019)
Paul Hiller - MLA-II certificant spearheads city-wide lubrication program (2018)
Improving creativity for engineers (2019)
Jeff O’Brien - Do you fit the bill? 8 crucial skills maintenance managers must have (2019)
Don Armstrong - Who makes a good maintenance manager? (2019)
Noria - Lube programme to avoid $2 million annual losses (2017)
Why Smart Manufacturing is a dumb idea
Elevating the status of lubrication personnel
Why train for machinery lubrication?
How to equip lube technicians for success (2015)
ICML certification (2018)
Why train for machinery lubrication? (2011)
You need a lubrication skill development programme
Why education is the secret to successful change (2016)
Increase training to improve results
TESTOIL webinar schedule
Getting the most from lubrication personnel (2005)

Last word

The machine and the lubricant can telegraph hints and signals to us in a variety of ways, but only if we are both tuned in and literate to their message. Tuned in means being vigilant and ubiquitous, like a detective, always looking for clues even when camouflaged from view. Literate means not only recognising the presence of the clue but also being wise to the meaning of its message and the corrective response.

Condition-based maintenance is based on identifying measurable criteria that allows the time to plan for early intervention on failures, thus helping to reduce catastrophic and secondary damage. The earlier you are able to detect the failure, the more time you will have to prepare the spares, ensure labour resources and communicate the need to everyone.

A best practice tends to spread throughout an industry after a success has been demonstrated. However, demonstrated best practices can often be slow to implement, even within an organisation. The three main barriers to adoption of a best practice are a lack of knowledge about current best practices, a lack of motivation to make changes for their adoption, and a lack of knowledge and skills required to do so.

Light reading

The term tribology was mentioned for the first time in 1966 in the Jost Report, a study commissioned by the British government to investigate damage from wear. The committee headed by Peter Jost (1921-2016), estimated that application of basic principles of tribology could save the UK economy approx. ₤515 million per annum (1966).

What is tribology (2018)
Tribonet - History of tribology (2016)
Tribonet - Ancient tribology artifacts looted?
The crude oil fractional distillation
Wikipedia - Rheology
Common sales myths
Engines
Micro fog machine lubrication (1965)
Riding the Film - 1937 Chevrolet engine lubrication (11 minute video)

joke

Dictator of Equatorial Guinea, Francisco Macias, banned the use of lubricants in the Malabo city power plant, claiming that he has magical powers. The plant exploded.

Now seriously

Some time ago the International Fluid Power Society produced a webinar on the prevention and management of fluid injection injuries. It cited a study by Snarski and Birkhahn, two emergency department doctors at the New York Methodist Hospital, which contained some very sobering statistics:
* Fluid injection injuries are relatively rare with around 600 incidences in North America per year. That's the good news. The bad news is it means your average emergency department doctor may not recognize the seriousness of the situation.
* High-pressure grease guns/systems account for 57% of injection injuries. Paint, hydraulic oil and similar fluids account for 18%. And diesel fuel injectors 14%.
* The overall incidence of medical amputation resulting from such injuries is 48%. But if the injection pressure is greater than 7000 PSI, the amputation rate approaches 100%.
* The average elapsed time between occurrence of injury and seeking medical attention is 9 hours. This is attributed to the apparent benign nature of initial injection, combined with a lack of awareness of the seriousness of this type of injury.
* Disturbingly, where 10 hours or more elapses between occurrence of injury and medical intervention, the amputation rate approaches 100%.
Bottom line: fluid injection injuries are medical emergencies which typically require surgical intervention to release the injected fluid and limit the tissue damage it causes. This is something everyone who works on or near hydraulic machines needs to be aware of.
Brendan Casey

Please click here to e-mail me any suggestions or addresses that no longer work. Thank you!
Petr Vavruch - member of SAIMechE
Certificate of SAIMechE membership
Petr Vavruch in 2018
The expert

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Quotes are from many different sources - sorry for not to be able to acknowledge them, thank you all!

感谢

Petr Vavruch: The correct lubricant

NEWS

SUBJECT LINKS FOLLOWING THE SECTIONS OF THE BOOK

Lubrication - general

Don't use the terrible slang "weight"!

TWC: Three-way catalyst, used for reducing toxic emissions from petrol engines

Ninety percent of lubrication professionals say a lack of attention has negatively impacted the reliability of equipment at their plant.

1. Three basic aspects of lubricating oils

According to hydraulic component manufacturer Danfoss, if a hydraulic system operates at 85 °C, oil life is just 12% of what it would be if the system operated at 60 °C. And if the system operates at 100 °C, oil life is only 3% of what it would be if the system operated at 60 °C.

Some antioxidants, such as butyl hydroxy toluene (BHT), will turn oil bright red when oxidizing during normal service. While not always cause for alarm, it is clear evidence that the antioxidant is depleting.

1.1 Viscosity, kinematic, dynamic, ISO VG

1.2 and 1.3 Viscosity of engine oils and automotive gear oils, SAE, multi-grade

In America, fortunately only there, they have a disgusting ignorant slang calling SAE numbers "weights", like "30 weight" or "10w30 weight". I suggest that you use it only if you want to show that you know NOTHING about lubricants.

Ford recommends using SAE 5W-50 viscosity grade for its GT-500 engine instead of the SAE 5W-20 or SAE 5W-30 used by other engines. Arup Gangopadhyay

1.4 Viscosity index, viscosity modifiers, viscosity-temperature chart, calculators

1.7 Viscosity-temperature chart, blending

1.5 Pour point, pour point depressant

1.6 Flash point and Noack volatility

1.8 Foam, entrained air and air release, defoamant

Cavitation is a violent condition typically in the suction of a pump leading to wear caused by air bubbles or water or oil vapour bubbles.

Bad article, confusing foam with air entrainment. Petr: Don't add defoamant unless you really have to.

1.9 Base stocks, saturates, aromatic hydrocarbons, API groups

Many of the benefits of high saturates Group II were discovered in use rather than being predicted, such as their much superior dispersant additive response in heavy-duty diesel applications.

1.9.1 What does 'synthetic' mean?

Synthetics - general

Petroleum-based mineral oils function very well as lubricants in 90 percent of industrial applications. However, they also have limitations depending on the type of base stock and additives used, the refining technology, and the operating conditions.

The formerly known manufacturer of Molykote lubricants has been Dow Corning, a joint venture between Dow Chemical and Corning Incorporated for over 73 years. In 2016 our parent company Dow Chemical took us over and last year we had a merger with Dupont. Mathias Sottong

Synthetics - usage

The estimated improvements for the overall energy savings from a friction perspective only between Group III and PAO are in the range of 0.7% to 1.4%.

1.9.2 Polyalphaolefins (PAO)

PAOs have inherently higher specific heats, so it will absorb more heat allowing the PAO-based lubes and the parts that they lubricate to run cooler.

Food-grade lubricants

(Beyond the scope of the book)

1.9.3 Other synthetic hydrocarbons

1.9.5 Polyalkylene glycols (PAG) (polar compounds)

Sludge and varnish in hydraulic controls of turbines is not a problem with PAG turbine oils owing to their high solubility. However, some PAG turbine oils cause sudden oxidative degradation, resulting from a decrease in anti-oxidants due to poor thermal stability of those PAG base oils.

1.9.6 Esters, amides, environmentally friendly lubes

Vegetable oils and biodegradable lubricants

(Beyond the scope of the book)

1.9.7 Naphthenics

1.10 Oil performance, performance additives

1.11 Water separability (demulsibility)

1.12 Supplemental ('proprietary') additives

REVISION 1

3.1 Engine oils, engine oil additives, ZDDP, fuel economy

Friction and wear

(Beyond the scope of the book)

Sludge, drain intervals, maintenance

(Beyond the scope of the book)

3.2 Engine oil specifications, API service categories

3.2 API service categories - diesel engine oils

Paccar does not allow use of API FA-4 oils in any of its MX or PX engines. By the end of March 2019, API has only licensed 100 FA-4 products. Trucks are able to get 1 to 2 percent better fuel economy using FA-4 oils.

3.3 and 3.4 Sulphated ash, TBN

3.5 ILSAC (International Lubricant Standardization and Approval Committee)

The Lubrizol Corporation announced that Lubrizol PV1510 engine oil additive technology, designed to meet the complex requirements of the ILSAC GF-6 specification, is ready (April 2019)

3.6 ACEA (Association des Constructeurs Européens d'Automobiles) and Equipment Manufacturers (OEM)

In the M111 fuel economy test, ACEA C5-16 has a requirement set at 3.0% which is 0.5% higher than C2-16 at 2.5% and significantly higher than C3-16 at 1.0%.

3.9 Two-stroke petrol engines

3.10 Outboard motor oils

3.11 Motorcycle oils

Ducati calls for the chain to be cleaned and lubed every 1000 km. Also adjust your chain. Every time you clean, check the slack and adjust as needed.

Electric vehicles

3.12 Gas engines

3.13 Marine engines and emergency power generation, marine lubes

British diesel locomotive engines use SAE 15W-40 engine oil in diesel locomotives for more than 30 years.

3.15 Gas turbines

3.16 Automotive gear oils for manual gearboxes and final drives

3.17 Limited slip differentials

3.18 and 3.19 Eaton (form. Fuller) and ZF-FreedomLine, Caterpillar

3.20 Allison

3.21 Total Acid Number (TAN)

3.22 Automatic transmission fluids (ATF)

3.23 Farm equipment oils, UTTO, STOU

September 2020: Oronite has achieved an important milestone by achieving one of the first approvals of a tractor hydraulic fluid (THF) additive offering that meets the new ZF TE-ML 05E specification.

3.24 Brake fluids

REVISION 2

5. Lubrication conditions, EHL, anti-wear, EP

Metal sulfite, or Molybdenum disulfide (MoS2), is widely used as an additive in solid lubricants because of its low friction properties and robustness. However, at low loads or resistance, it shows excessive wear and higher friction.

6. Industrial gear oils

Overfilling a gearbox sump can be just as damaging as underfilling. Overfilling may cause air entrainment and foam, overheated oil, and leakage due to overflow. Over time, oxidation may also occur due to increased temperatures and exposure to air.

Ford recommends using SAE 5W-50 viscosity grade for its GT-500 engine instead of the SAE 5W-20 or SAE 5W-30 used by other engines.
Arup Gangopadhyay

The formerly known manufacturer of Molykote lubricants has been Dow Corning, a joint venture between Dow Chemical and Corning Incorporated for over 73 years. In 2016 our parent company Dow Chemical took us over and last year we had a merger with Dupont.
Mathias Sottong

Paccar does not allow use of API FA-4 oils in any of its MX or PX engines.

By the end of March 2019, API has only licensed 100 FA-4 products.

Trucks are able to get 1 to 2 percent better fuel economy using FA-4 oils.